GCMS analysis results for sample AE08324, May 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08324.D vial: 11 Acq On : 19 Apr 2002 5:58 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 2-Propanone, 1,1,1-trichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 6.12 0.74 ug/1 1042940 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 40 2 Acetamide, N-methyl- 73 C3H7NO 000079-16-3 9 3 1,3-Dioxolane-2-ethanol, 2-methy... 174 C8H14O4 068039-72-5 9 4 1,2-Propanediol, 2-acetate 118 C5H10O3 006214-01-3 9 Abundance Scan 517 (6.117 min): 08324.D (-512) (-) m/z 43.05 100.00% 43

5000 73

"PT— ' ■1 । 5.80 6.00 '11'1 ■11 ■11111• T -Hr 55 63 83 97 ‘T—— 1, 11712 1111T1/10/1/1/"11111‘1TC"‘TTTTTTrTEIIIT m/z 73.10 6.20 6.40 45.40% m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #3877: 2-Propanone, 1,1,1 -trichloro- 43

5000 5 80 6.00 6.20 6.40 m/z 125.00 10.14% 15 27 35 , , 53 63 73 83 I" I ■-r- TT 9/ 117 125 +TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT m/z->_____ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #109186: Acetamide, N-methyl- 3p 43 73 ■ ■ 1 । ' 1 1 1 । ■ ■ ■ ' । r r ■ ■ । ■ ■ 1 1 i 5 80 6.00 6.20 6.40 5000 58 m/z 97.00 6.44%

n/z~> ........... 1 10 20 30 44T 60 70 80 90 100 110 120 130 140 150 160 40 50 TITTTTTTTLTTTTLTTTTTTTTTIBTLPTETTTIT

Abundance #7235:1,3-Dioxolane-2-ethanol, 2-methyl-, acetate 43 5.80 6.00 6.20 6.40 87 m/z 83.00 6.17% 5000 99 55

m/z-> AL 27 " I " ■ r i lpe ' ‘‘114 10 20 30 40 50 60 71 - TTI +115 111 111 132 159 I ■1111 • • > > 111'' i ■ ■ 70 80 90 100 110 120 130 140 150 160 5.80 AAAAAA 6.00 6.20 6.40

08324.D SCAN020418.M Fri May 03 09:04:37 2002 Page 6

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