GCMS analysis results for sample AE07769, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07769.D Vial: 23 Acq On 5 Apr 2002 3:26 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.59 0.31 ug/1 201992 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 2 2 Acetaldehyde, O-methyloxime 73 C3H7NO 033581-43-0 2 3 1-Propanamine, N,2-dimethyl-N-ni... 116 C5H12N20 034419-76-6 2 4 N-Ethylformamide 73 C3H7NO 000627-45-2 1 Abundance Scan 427 (5.588 min): 07769.D (-417) (-) m/ z 43.10 100.00% 43

5000 73 1 i 1 ' 1 ' i ' 1 1 ■ i ' ' 125 5.20 5.40 5.60 5.80 6.00 49 84 | 01 ' I ‘ ‘ I ' ' ' ' I ' ' ' ' I 1 ' 1 1 1 1 ■i'■'■i1■■1i1111 i 1 11 1 1 1 1 ■ r i 1 1 1 1 i 1 11 ■ i 1 1 m/ Z 73.10 23.47% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3877: 2-Propanone, 1,1,1-trichloro- 43

5000 1 । ■ 1 1 i 1 ■ 1 1 i 1 1 1 1 i 1 1 5.20 5.40 5.60 5.80 6.00 m/z 125.00 10.83% 15 07 I 01 TIP27 36 . ,49 55 63 1 1 ''I ■ 1 1 ' I'1 76 83 91 97 110117i 1125 1 i 1 ' 1 ‘ i 1 1 11 1* ■ ''''i 1 1 1 1 i ■ 1 ■ ■ । ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3241: Acetaldehyde, O-methyloxime 42 1 1 i 1 ■ ■ 1 i ■ ■ 5.20 5.40 5.60 5.80 6.00 5000 m/ z 47.00 8.50% 29 73 58 Of ■ i 1 1 1 ■ i 1 — II, > | i > r i i i — it I i | I i i I । i i i i । t i t i — , > > । t i i t । i r n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3322:1-Propanamine, N,2-dimethyl-N-nitroso- 1 ' i 1 ' 42 5.20 5.40 5.60 5.80 6.00 m/z 84.00 3.10% 5000 30 "YN"WMM*/MMpnsoyol 56 73 1 I 50 1 67., | 84 99 116 0 1 1 i 1 1 1 1 i 1 ■ । |-i । ■ T ] I IJ • । |' I 'I I । ‘| ' I I I ' I | 'l I I I | I'll 1 ']■ | I I | '| I | I I | I I | I | I I J J | TT

n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.20 5.40 5.60 5.80 6.00

07769.D SCAN020403.M Wed Apr 10 11:20:28 2002 Page 4

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