GCMS sample preparation log, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020515\0513LB2.D Vial: 4 Acq On : 15 May 2002 2:47 pm Operator: Nefliu Sample : 05/13 lab blk Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 3,5-Ethanoquinolin-10-ol, d... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.26 ug/1 25407 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,5-Efthanoquinolin-10-ol, decahy. . . 209 C13H23NO 021041-43-0 59 2 Anthracene, 1-methyl- 192 C15H12 000610-48-0 53 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 53 4 1H- Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 1000196-69-5 40 Abundance’ Scan 4768 (31.094 min): 0513LB2.D (-4758) (-) m/z 192.10 100.00% 192

5000

44 7Q |^118 1J61 30.80 31.00 31.20 31.40 11" । 11 ’ । 1l । ‘| i-i । ... 478 m/z 193.10 19.55% nz-> 0 50 100 150 200 250 300 350 400 450 Abundance #81097:3,5-Ethanoquinolin-10-ol, decahydro-1,7-dimethyI-,... 1912 ..........................................

5000 44 166 30.80 31.00 31.20 31.40 m/Z 146.00 13.97% 70 96 A I lU 4 4 ill 122 m/z—> 0 r 50 4 -150 100 1- 200 1, 250 300 350 400 450 Abundance #125854: Anthracene, 1-methyl- 192 I........Ill....... 30.80 31.00 31.20 31.40 5000 m/z 191.10 13.12%

82 165 16 39 ,1..1115139 1 miz-> 0 50 100 150 200 250 300 350 400 450 Abundance #81034: Anthracene, 2-methyl- • 1 I ■ ■ ' 1 i ' ' ' ■ i ' ' 192 30.80 31.00 31.20 31.40 m/z 160.10 12.70% 5000

82 165 1439 1-1,1115139 1 i ' ■ 1 ■ i ' 1 ■ ' i 1 1 ■ ■ r1 1 1 Id । । । । । > ' ' I ' 1 1 1 i ' ' ■ i * 1 ' 1 । ■ m/z-> 0 50 100 150 200 250 300 350 400 450 30.80 31.00 31.20 31.40

0513LB2.D SCAN020507.M Thu May 16 14:44:12 2002 Page 5

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