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GCMS analysis results for sample AE10247, May 28, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE10247 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024907–000024914

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020509\10247.D Vial: 25 Acq On : 10 May 2002 10:21 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.34 ug/1 41718 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 81 2 Benzene, 1-(1-cyclohexen-l-yl)-4.. . 188 C13H160 020758-60-5 49 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 47 4 Pyrolo[2,3-b]indole, 1,2,3,3a,8. . . 188 C12H16N2 004089-16-1 46 Abundance? Scan 4913 (31.946 min): 10247.D (-4907) (-) m/z 188.15 100.00% 188

5000

80 94 31.60 31.80 32.00 32.20

n/z->20 43 66 10119 1 1 1 1 ' ■ ■ i '■ ■ ■ 1 1 1 1 1 1 '1 ' 40 60 80 100 120 140 8 160 180 200 224 220 ■ ' i ■ ' 1 ■ i ' ' m/ z 184.10 20.44%

Abundance #79826: Anthracene-d1 0- 1(18

5000 31.60 31.80 32.00 32.20 m/z 80.05 19.35% 80 94 160 1 17 30 42 52 66 ,l198118.132146,4170L —— mtz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #79791: Benzene, 1-(1-cyclohexen-1-yl)-4-methoxy- 188

31.60 31.80 32.00 32.20 5000 160 m/z .94.05 19.14%

91 115 129 145 173 41 51 65 77 1 1 I । । । । I1'1' 1s 11, , ll . 1 1.,192 ,4,44 4 , Mit nz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 31.60 31.80 32.00 32.20 m/z 187.20 13.29% 145 5000

117 41 51 , 63 77 89 -(no 130

tJz-> ' 1 1 1 1 1 1 "i 20 40 rlt , [ls ,. .,111,1, m , 60 80 — ! l , | "I 100 120 140 kIepcinn 159 173 160 —)180i ■ 200 220 31.60 31.80 32.00 32.20

10247.D SCAN020507.M Tue May 14 14:26:47 2002 Page 5

NYC-WTC_000024913

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NYC-WTC_000024913Source: NYC Law Department, mirrored locally

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