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GCMS quantitation results for sample AE10301, May 2002

Machine-extracted title · confidence 90%

Laboratory report of GCMS analysis for sample AE10301 conducted on May 28, 2002.

NYC-WTC_000024915–000024926

Folder label: “GCMS X 5/14/02 A 5/17/02

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Scanned page image, NYC-WTC_000024925
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\10301.D Vial: 24 Acq On : 17 May 2002 8:04 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.35 ug/1 24512 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diO- 188 C14D10 001719-06-8 64 2 Phenanthrene-diO 188 C14D10 001517-22-2 59 3 Benzene, 1-(1-cyclohexen-l-yl) -4... 188 C13H16O 020758-60-5 53 4 ^-Isoxazoline, 3-mesityl-5-pheny... 297 C18H19NOS 1000164-78-1 53 Abundance Scan 4916 (31.964 min): 10301 .D (-4907) (-) m/z 188.20 100.00% 168

5000 94 . I r . . I I IT | I 1-! ! | I I ! ! | |

42 51 66 80 160 |, 31.60 31.80 32.00 32.20 104 ' i "'11" " i" " i' ■ " i'" " i " । ■ i" r ■ I ■1'' i l'l ■ ' i" ■ ‘ i" " i " ' ■ i " " r "' i " ■11" " i" " i ■1171 ■" ■ m/ z 94.10 26.94% miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/ z 184.2 0 20.77% 80 94 160 , , 66 17 30 42 52 ' 1 J 108118 'I "'I 11 11 11 1 I I I 111 11 11 I 11 IT1 132.146, 1*.179179l..1 n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

31.60 31.80 32.00 32.20 5000 m/z 187.20 15.36%

80 94 160 30 42 52 66 m/z-> TmWWTITTNTTTTTTTTTT —+l+198118..132.146—44179179l 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79791: Benzene, 1-(1-cyclohexen-1-yl)-4-methoxy- 1(18 31.60 31.80 32.00 32.20 m/z 189.05 13.98% 5000 160

115 129 145 173 91 41 51 65 77 ' I / — IT | I I I I | ! I I I | I

/z—> ----- T102 II I I AH Hrpen 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 . .... 4- 31.60 31.80 32.00 32.20

10301.D SCAN020507.M Fri May 17 10:51:28 2002 Page 7

NYC-WTC_000024925

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NYC-WTC_000024925Source: NYC Law Department, mirrored locally

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