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GCMS analysis page for sample AE11571, May 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE11571 showing unknown compounds and surrogate recovery data from May 29, 2002.

NYC-WTC_000025613–000025623

Folder label: “GCMS X 5/17/02 A 5/16/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11571.D Vial: 24 Acq On : 22 May 2002 7:05 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.33 ug/1 36057 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dl0- 188 C14D10 001719-06-8 72 2 Phenanthrene-diO 188 C14D10 001517-22-2 45 3 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 25 4 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 9 Abundance Scan 4914 (31.952 min): 11571. D (-4907) (-) m/z 188.20 100.00% 188

5000

94 156 80 42 54 66 130 146 31.60 31.80 32.00 32.20 0 mmmHH . ......... ........I"' lj_____ I’11 ‘ I m/z 94.05 19.73% mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/z 184.20 18.17% 80 94 160 17 30 42 52 66 108118 132 146 ,|| 170179 ■1 • i111 ■ r1'1111 ■1111 ■ 1111>। ■'11 , 0 TTNTTnTT mfz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 1(8 1 1 I 1 1 11 I 1 31.60 31.80 32.00 32.20 5000 m/Z 156.10 16.34%

94 80 160 30 42 52 66 11 108118 132 146 ,|,I 170179.1,1 0- I" " 111" 11'" 11'1' 111" I"111" H 1"11TTTT ‘I m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79714: Pentacyclo[8.4.0.0(3,7).0(4,14).0(6,11)]tetradecane 1(8 31.60 31.80 32.00 32.20 m/z 80.00 13.58% 5000 79 91 117 131 145 159 173 /........................................ .67 .106

miz—> 27 41 55 0 -—H—l— +lH++H+H U 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

11571.D SCAN020521.M Fri May 24 09:50:00 2002 Page 5

NYC-WTC_000025621

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NYC-WTC_000025621Source: NYC Law Department, mirrored locally

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