GCMS analysis page for sample AE11571, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11571.D Vial: 24 Acq On : 22 May 2002 7:05 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 4-Hydroxy-3,5-dimethylcinna... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.30 ug/1 32572 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 53 2 2,5-Dih drophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 53 3 5H-Tetr azole-5-thione, 1,4-dihyd... 192 C8H8N4S 1000142-22-5 37 4 [2,2'-Bifuran]-3-carboxylic acid... 192 C1OH804 005905-07-7 32 Abundance Scan 4767 (31.088 min): 11571.0 (-4753) (-) m/z 192.10 100.00% 192

5000

T-FI--IT 51 70 | 365 30.80 31.00 31.20 31.40 0 ’ I ‘ ' 111lm" I' "l ' ill I'1 ' i ■ ■ " i' " ' i1" ' I " " i " " i ■ " ri " " I " " m/z 191.10 31.06% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid 192

5000 I.............. 1 1 ■ । ' 1 1 1 i ' 1 ■ 1 i 1 ■ 30.80 31.00 31.20 31.40 175 m/z 96.00 20.51% 63 89 +4lyr+rh 117 145 Mira I....................................................... 45 I 0- H,, A । ■ ‘111 ‘1" ।"111' ■ ■' । ■ ■ ■ • ।" ■ ■ । ■' ■ ■ ।1"1111' ■ । ■1 n/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundances #80965:2,5-Dihydrophosphole, 3-methyl-1 -oxo-1 -phenyl- 192 164 ......III.,..I... 30.80 31.00 31.20 31.40 5000 99 33 115 m/z 82.10 15.46% 47 77 146 0 -47+ । + 4 H + 411' [ 44 AH ■ 'i'1 111" ' i ‘' i" " i1" 11" 111" " 11" 1111" i1111 n/z-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 #80933:5H-Tetrazole-5-thione, 1,4-dihydro-1 -methyl-4-phenyl- 135 192 ..... Ill ,l.... 30.80 31.00 31.20 31.40 m/z 146.20 13.75% 77 5000 51

I 104 1 HLp44,44 #4 11'"163I ’1" I • > 111111111111111T1911’1110—1——00——331"11107T oV /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 30.80 31.00 31.20 31.40

11571.D SCAN020521.M Fri May 24 09:50:00 2002 Page 4

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