GCMS analysis results for sample AE08427, May 2002

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Laboratory report documenting GCMS analysis of sample AE08427 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048182–000048194

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08427.D Vial: 14 Acq On : 19 Apr 2002 8:56 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 4 4-Hydroxy-3,5-dimethylcinna ... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

31.09 0.35 ug/1 772249 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 53 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 4 Anthracene, 9-methyl-_______________ 192 C15H12 000779-02-2 40 Abundance Scan 4768 (31.094 min): 08427.D (-4751) (-) m/z 192.10 100.00% 192

5000 40 ‘ I’’ 82 96 . 146 160 30.80 31.00 31.20 31.40 55 | 70 | 118 । III|IIII|I ' i ‘■ i'' ''I 1 ' | 1 | ' I 1 । I I I I | I N'l | I 1 I 1 | 1 I I I | I I I I | I r | | | | I'l'i | 1 ! 1 H m/ z 40.10 —WYW-WwwOWwAR 32.80% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid 192

5000 30.80 31.00 31.20 31.40 89 175 rn/z 191.10 22.18% 63 117 145

/z-> .. 145453411 77 105 11 +-HH— TTTTu 135 163 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TT’

Abundance #81033: Phenanthrene, 9-methyl- 192 ................... . ......................... 30.80 31.00 31.20 31.40 5000 m/z 193.10 16.24%

96 29 39 51 63 J 75 83115 126 139 152 165 176 ’I’*’’e’’*’p*uuutt-)"vd"n"kua i''111'11' 1111111 rT I" . . ...... 11111 |'i । > > । l TPTTT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 30.80 31.00 31.20 31.40 161 m/z 146.10 14.02%

5000 A 77 91| 22 121I 138 149 177 103 52 64 I 11 • " • r " ' 11111 r 1 r 11111111111 1,..... . ..... I .I,, l..... .... 1.... 1 T-rp- m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

08427.D SCAN020418 .M Thu May 02 15:34:25 2002 Page 6

NYC-WTC_000048191

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GCMS analysis results for sample AE08426, May 2002 · Box DEP Box 27

NYC-WTC_000048169

Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.

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