GCMS analysis page for sample AE11571, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\02052111571.D Vial: 24 Acq On : 22 May 2002 7:05 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 9-[6-Hydroxyhexyl]hypoxanthine Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 40.51 0.23 ug/1 21895 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 9- -Hydroxyhexyl]hypoxanthine 236 C11H16N4O2 1000213-13-8 18 2 1, -Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 10 3 5-Fluoro-2-methylphenyl isothioc... 167 C8H6FNS 1000134-57-2 9 4 Heptanal 114 C7H140 000111-71-7 9 Abundance Scan 6370 (40.507 min): 11571 .D (-6360) (-) m/z 149.10 100.00% 70 149 167 44 281 86 5000 109 236 258 304

40.20 40.40 40.60 40.80 8 '11111111 i'' 17 11' ■ ■ I’ i'1'' i'1 ' ‘ i ■' ■11 ■' T‘011"‘1111111T m/ z 70.20 99.80% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #66979: 9-[6-Hydroxyhexyl]hypoxanthine 149

5000 191 ■ • i ■ ■ 1 1 17 i 163 236 109 40.20 40.40 40.60 40.80 41 55 205 m/z 166.90 177 95.70%

miz-> 0- TT-p- 20 — 1 81 94123.44 T11!'1,11111′1’’’ ′′′′′′′ 11 1111111 ‘ I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ii 4. | 219

Abundance #67064:1,2-Benzenedicarboxylic acid, mono(2-ethylhexyl) este 149

40.20 40.40 40.60 40.80 5000 m/ z 44.00 81.05% 70 167 41 55 9: 93 112 0- 1117 el Ah4, L—,1132.4 , 185199213228242256 278 • 11 ■ ■ < I • > ■ >‘11 > ■1 j ■ । -1 < < < ■ i ■ ■ • ■ j ■ • ■ ■ । mz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #73316:5-Fluoro-2-methylphenyl isothiocyanate 167 40.20 40.40 40.60 40.80 ' m/ z 281.30 70.31% 5000 135 57 83 107

I 39

0 15,444,4414444444121— 111 11'1" i1 i 1''' i ■1'' i 111 TIT ' 1 1 ' ' 11 | 1 1 1 ' | ' । ‘ | n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 40.20 40.40 40.60 40.80

11571.D SCAN020521.M Fri May 24 09:50:00 2002 Page 6

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