GCMS analysis results for sample AE10246, May 28, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020509\10246.D Vial: 24 Acq On : 10 May 2002 9:21 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 7 15-Tetracosenoic acid, meth... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 36.95 1.05 ug/1 116076 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 15-Tetracosenoic acid, methyl es... 380 C25H4802 002733-88-2 74 2 Oxacyclohexadecan-2-one! 240 C15H28O2 000106-02-5 72 3 1-Dodecanol 186 C12H260 000112-53-8 59 4 1/-Hexadecanol 242 C16H340 036653-82-4 52 Abundance Scan 5765 (36.952 min): 10246.D (-5759) (-) m/ z 55.10 100.00% 55

5000 83 MM MrYMMWa"? । । । । । i r i । i > Ta li 111 36.60 36.80 37.00 37.20

m/z-> 414421—A7 39 ill U ■ ■ r ■ " i ■' 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 m/ z 69.05 54.03% Abundance #111261:15-Tetracosenoic acid, methyl ester, (Z)- 55

83 5000 36.60 36.80 37.00 37.20 m/z 83.10 47.21% . 111 3!

/z-> mH ITT 138157,181207.. ................... 349 n >' I * |T> >Y | -| > 1 । 111 । > । । । 11 । ■ > 11 j । ■ 11 11 ■ ■ । । > > । ■ 11111111 11 11 r ■ i [ । ri 11 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #111517: Oxacyclohexadecan-2-one 55 AAMads 36.60 36.80 37.00 37.20 5000 m/Z 97.20 40.27% 83

28 I I110 12 mfe-> -+H 4441A0744 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #13544:1-Dodecanol AM MAAMps 55 36.60 36.80 37.00 37.20 83 m/z 43.10 38.89%

N 5000 29 111 140 — p-T4 '111 ■ ‘ , 168 ‘MWA/y /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 36.60 36.80 37.00 37.20

10246.D SCAN020507.M Tue May 14 14:26:42 2002 Page 9

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