GCMS quantitation results for sample AE10246, May 2002

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Laboratory report of GCMS analysis for sample AE10246 conducted on May 28, 2002.

NYC-WTC_000024871–000024882

Folder label: “GCMS X 5/14/02 A 5/17/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\10246.D Vial: 22 Acq On : 17 May 2002 6:05 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.32 ug/1 23827 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

_ 1 Anthracene-dlO- 188 C14D10 001719-06-8 64 2 1,2-Bis(2-hydroxyphenyl)ethylene... 376 C24H28N2O2 1000187-13-2 42 3 Pyyrolo[2,3-b]indole, 1,2,3,3a,8... 188 C12H16N2 004089-16-1 38 4 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 33 Abundance Scan 4915 (31.958 min): 10246.D (-4907) (-) m/z 188.15 100.00% 188

5000 — 80 54 100 160 31.60 31.80 32.00 32.20 341 1' I ITT) 1 1 1 v - " r " ' l " " i" " r' " i" " r "1 r" 1111"111" " I" m/z 189.10 23.25% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/z 80.00 22.08% 17,42.46444114132/1.4 n/z-> Abundance • •i" i*‘•i" 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #79831:1,2-Bis(2-hydroxyphenyl)ethylenediamine, N,N’-bis(... 188 i" " i*" ■> ■■ ■■ i i ’ • * • i" ' I J I.. _ 31.60 31.80 32.00 32.20 5000 m/z 184.00 19.58%

41 77 94 I _ I I I 121 145 171 ipt, 4 ph ri Ar vheth A r hh/ 210 238255 '‘ i"1 ■ i ■"11 ■ ‘ 293 377 i'"' 11'" i ■"' i" "i" " i"" i" m/z-> 20 40 60 80 100 120 140160180 200 220 240 260 280 300 320 340 360 380 Abundance #79762: Pyrrolo[2,3-b]indole, 1,2,3,3a,8,8a-hexahydro-3a,8... 188 ITI11‘I1II*1* 144 31.60 31.80 32.00 32.20 m/z 92.20 17.16% 5000

...... .. 171 441 ‘‘I‘‘AAI‘‘‘+I‘AAAI****I‘‘‘AA‘**I‘I‘GIUIIITTI‘I m/z—> 20 40 60 80 100120 140160 180 200 220 240 260 280 300 320 340 360 380 31.60 31.80 32.00 32.20

10246.D SCAN020507.M Fri May 17 10:48:22 2002 Page 7

NYC-WTC_000024881

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GCMS quantitation results for sample AE10247, May 2002 · Box DEP Box 18

NYC-WTC_000024896

Laboratory report of GCMS analysis for sample AE10247 conducted on May 28, 2002.

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