GCMS analysis results for sample AE08489, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020419\08488.D Vial: 25 Acq On : 20 Apr 2002 7:45 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.31 ug/1 607713 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 86 2 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 59 3 4-Methyl-2-(3-fluorophenyl)pyrim... 188 C11H9FN2 076128-66-0 45 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 45 Abundance Scan 4916 (31.963 min): 08488.D (-4907) (-) m/z 188.15 100.00% 188

5000 1. —I 0 40 94 ‘I 66 31.60 31.80 32.00 32.20 , eri— 1132790 547 i ' ■ ■ ■ i ' ■ ' ■ i ■ ■ ■ ■ i ' ■ ■ ■ i ' 1 ■ ' i ■ ■ ■ ■ i ■ ■ ' ' 'i ‘ m/z 40.10 19.22% miz-> 0 50 100 150 200250300350400450500550 Abundance #79826: Anthracene-d10- 108

5000 31.60 31.80 32.00 32.20 m/z 94.10 15.74%

niz-> 6 +40,6144122’414 250 “300 350 400 450 500 550 50 100 150 200 Abundance #79821: Selenide, ethyl 1-methyI-1-penten-3-ynyl 108 *F - 31.60 31.80 32.00 32.20 5000 m/z 184.15 11.36% 79 159

mfz~> 0 ...244 50 100 150 200250300350400450500550 Abundance #79744:4-Methyl-2-(3-fluorophenyl)pyrimidine T! 108 31.60 31.80 32.00 32.20 rn/z 189.10 10.78%

5000 121

67 94

/z—> 0 39 1 V - '' l t 11 50 100 150 200 1461 250 300 350 400 450 500 550 II ------- 31.60 31.80 32.00 32.20

08488.D SCAN020418.M Thu May 02 12:03:41 2002 Page 6

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