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GCMS results for sample AE11482, May 29, 2002

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Laboratory report of GCMS analysis for sample AE11482 conducted on May 29, 2002.

NYC-WTC_000022588–000022597

Folder label: “GCMS X 5/17/12 A 5/21/02

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NYC 9/11 Public Portal Document Llprary search Compound Report Data File : C:\MSDCHEM\l\DATA\020521\11482.D Vial: 16 Acq On : 21 May 2002 11:11 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.34 ug/1 33997 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 83 2 3-Quinolinecarbonitrile, 1,2,3,4... 188 C10H8N2O2 022384-05-0 38 3 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 25 4 1,2/Bis(2-hydroxyphenyl)ethylene... 376 C24H28N2O2 1000187-13-2 16 Abundance Scan 4916 (31.963 min): 11482.D (-4906) (-) m/z 188.20 100.00% 188

5000 94 66 80 158

miz-> 40 52 0 ---------- lL, TTTTTTTTTTTTT 108 132 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31 60 31.80 32.00 32.20 m/z A 94.00 33.40% Abundance #79826: Anthracene-d1 0- 188

5000 31,60 31.80 32.00 32.20 80 94 160 m/z 66.10 27.21% 17 30 42 52 ° | J 108118 132 146 II 17017911 I 0 TpmmmmmHt ‘I z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79679:3-Quinolinecarbonitrile, 1,2,3,4-tetrahydro1-hydr... 188

18 31 60 31.80 32.00 32.20 93 128 172 5000 117 m/z 189.30 22.48% 142

27 104 161 O-p ITT — I..... n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance। #79821: Selenide, ethyl 1-methyl-1-penten-3-ynyl "I 188 31.60 31.80 32.00 32.20 m/z 158.10 19.61% 5000

79 145 159 , 173 I । / . ( T । . , , , । , I , । , 91 107 119 131 0\| . .. . | . I ip-11 11 rn 11 I ni 11II 111 I I

n/z—> TPTTTTTT —lmHl# 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 -m-rj

31.60 31.80 32.00 32.20

11482.D SCAN020521.M Fri May 24 09:38:48 2002 Page 5

NYC-WTC_000022596

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NYC-WTC_000022596Source: NYC Law Department, mirrored locally

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