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GCMS analysis results for sample AE11153, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11153 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024484–000024494

Folder label: “GCMS X 5/13/02 A 5/16/02

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Scanned page image, NYC-WTC_000024493
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NYC 9/11 Public Portal Document Llbrary search compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11153.D Vial: 19 Acq On : 16 May 2002 5:35 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.36 ug/1 39383 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

- 1 Anthracene-diO- 188 C14D10 001719-06-8 64 2 Phemanthrene-dlO 188 C14D10 001517-22-2 59 3 1H-Purine, 2,6-dichloro- 188 C5H2C12N4 005451-40-1 32 4 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 32 Abundance Scan 4915 (31.958 min): 11153.D (-4905) (-) m/z 188.20 100.00% 188

5000 94 80 158 52 66 31.60 31.80 32.00 32.20 | 306 — '1' i' I I I ’ ‘1 ' I TII ■' i ■ ‘' i ''' ■ i IT I ' ' ' m/ z 94.20 34.62% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79826: Anthracene-d10- 188

--- 5000 31,60 31.80 32.00 32.20 m/ z 92.20 19.50% 80 94 160

miz-> 20 40 5/Xi X j.1,4.. 4... 60 80 ■ ■ i ■' ■ ‘ i ■ ■ ■ ■ i'' ■ ■ i' ■ ■ ■ i ■ ■ 100 120 140 160 180 200 220 240 260 280 300 Abundance #79827: Phenanthrene-d1 0 188

31.60 31.80 32.00 32.20 5000 m/z 158.00 18.26%

80 94 30 52 66 —Imuniputti — , i ll 198. ! 132146 ‘11''' ■ 11 ’111 I ' '1 ' I mz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79846:1 H-Purine, 2,6-dichloro- 188 31.60 31.80 32.00 32.20 m/ z 184.00 17.84% 153 5000

92 47 65 . 11111. ।. l, h । 118 134 +HMM mm Tl/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 31.60 31.80 32.00 32.20

11153.D SCAN020507.M Thu May 16 09:30:33 2002 Page 6

NYC-WTC_000024493

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NYC-WTC_000024493Source: NYC Law Department, mirrored locally

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