Laboratory report documenting GCMS analysis of sample AE11153 conducted on May 22, 2002, including surrogate recovery data.
NYC-WTC_000024484–000024494Folder label: “GCMS X 5/13/02 A 5/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document LIbrary searen compound Report Data File : C:\MSDCHEM\1\DATA\020515\11153.D Vial: 19 Acq On : 16 May 2002 5:35 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ************************************************** * * * * * * * * * ********** Peak Number 3 2,4-Diamino-6-(hydroxymethy... Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T. 31.08 0.32 ug/1 35363 Phenanthrene-dl0 31.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2,4 amino-6-(hydroxymethyl)pte... 192 C7H8N6O 000945-24-4 40 2 Thiocyanic acid, 2-benzothiazoly. . . 192 C8H4N2S2 006011-99-0 38 3 3-(2-Methoxy- 5-methylphenyl)acry... 192 C11H12O3 103986-76-1 38 4 [2, Bifuran]-3-carboxylic acid... 192 C1OH804 005905-07-7 36 Abundance Scan 4766 (31.082 min): 11153. D (-4756) (-) m/z 192.00 100.00% 192 ................ )
5000
■ ■ । ■
43 52 7082 96 120 134 146 160 10 30.80 31,00 31.20 31.40 " i " " r ' " i" i7" ■ i1 ll’’ | ‘ ' I । * ' I | " 1 1 | 1 TTP I I ! | I I I I [ ! 1 I I |'! I HTT I I I I I I | I I I I | I M17 I m/ Z 82.00 16.48% 1" i1 mfz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125821:2,4-Diamino-6-(hydroxymethyl)pteridine 43 1912 163
5000 1. ...in.. 28 30.80 31.00 31.20 31.40 53 .. 68 146 175 m/z 160.10 13.04% 92 106 121 133
nz-> - ----- .77, 'rrrTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4MHHHH Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 19/2 i... ' ' ' I ' ‘ ' 1 I 1 v " 11 " 30.80 31.00 31.20 31,40 5000 m/Z 193.20 10.27%
45 TTUEDTTOTDTTTTTTTTT 1.. ,.90 108 122 134 148 160 1" 11 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80954:3-(2-Methoxy-5-methylphenyl)acrylic acid 161 192 30.80 31.00 31.20 31.40 m/ z 76.20 9.37% 5000 105 77 132 39 51 65 91 115 , 145
•n/z-> ----- J 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 .. .... mP U 175 ’r-rl 1 1 1 1 I 1 30.80 31.00 31.20 31.40
11153.D SCAN020507.M Thu May 16 09:30:31 2002 Page 5
NYC-WTC_000024492
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NYC-WTC_000025613
GCMS analysis report for sample AE11571 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022598
Laboratory report of GCMS analysis for sample AE11566 conducted on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024652
GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022539
Laboratory report of GCMS analysis for sample AE11426 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024896
Laboratory report of GCMS analysis for sample AE10247 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025568
GCMS analysis report for sample AE11567 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022516
Reference standard analysis report for nitrosamines and benzene derivatives in sample AE11424 analyzed May 17-21, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025592
GCMS analysis report for sample AE11569 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024813
Laboratory report of GCMS analysis for sample AE10243 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024706
Laboratory report documenting GCMS analysis of sample AE11281 conducted on May 22, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046159
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10130 on May 17, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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