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GCMS analysis results for sample AE10302, May 10, 2002

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Laboratory report documenting GCMS analysis of sample AE10302 conducted on May 10, 2002, including surrogate recovery data.

NYC-WTC_000024946–000024952

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document Library searen compound Report

Data File : C:\MSDCHEM\l\DATA\020509\10302.D Vial: 27 Acq On : 10 May 2002 12:19 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.33 ug/1 39855 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diO- 188 C14D10 001719-06-8 58 2 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 37 3 2-A2-(Phenylselenyl)propyl]isoin... 345 C17H15NO2Se 1000210-81-6 37 4 Nickel , di-.mu. -carbonylbis ( .eta. . . 302 C12H10Ni2O2 012170-92-2 35 Abundance Scan 4915 (31.958 min): 10302.D (-4908) (-) m/z 188.10 100.00% 188

5000 80 158 JA.......... . m/z-> 52 TTT 50 42.‘2L1 100 150 200 250 300 350 399 400 450 478 31.60 31.80 32.00 32.20 m/ z 80.00 23.42% Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/ z 15 8.20 20.13% , 49 66 i 94 , 160 I 17,42., 1.132 4 .................. ......................... । m/z-> 50 100 150 200 250 300 350 400 450 Abundance #79745:4-Methyl-2-(4-fluorophenyl)pyrimidine 108 121 31.60 31.80 32.00 32.20 5000 m/z 94.20 19.67%

67 94 TTT 39 J,., k , — 146 n/z-> 50 100 150 200 250 300 350 400 450 Abundance #79751:2-[2-(Phenylselenyl)propyl]isoindole-1,3-dione 108 31.60 31.80 32.00 32.20 m/z 160.10 17.93% 5000 41 130 77 160 345 TT | 105 h t, rA-1 M, , j . I h + 4 217239 272 314 , /............ /z—> 50 100 150 200 250 300 350 400 450 31.60 31.80 32.00 32.20

10302.D SCAN020507.M Tue May 14 14:26:59 2002 Page 4

NYC-WTC_000024951

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NYC-WTC_000024951Source: NYC Law Department, mirrored locally

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