GCMS analysis results for sample AD31644, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31644 including unknown compounds and surrogate recovery data.

NYC-WTC_000049990–000050007

Folder label: “GCMS X 1/3/02 A 1/17/02”

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NYC 9/11 Public Portal Document LIbrary searen compound Report Data File : C:\MSDCHEM\1\5973N\02JAN17\31644.D Vial: 4 ' Acq On : 17 Jan 2002 5:19 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.33 ug/L 213554 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 87 3 Phenanthrene-diO 188 C14D10 001517-22-2 86 4 Anthracene-D10 188 C14D10 000000-00-0 72 Abundance Scan 1699 (22.771 min): 31644.D (-) m/z 188.10 100.00% 188

5000 .......... ............ 94 22.40 22.60 22.80 23.00 23.20 n/z-> 42 54 66 80 0 — tlanajlhanpam 30 40 50 60 70 80 m 132 90 100 110 120 130 140 150 160 170 180 190 160 m/z 94.05 17.63% Abundance #84502: Anthracene-d10- 1(18

5000 . । .... । . rf . । < i . . । , . . . । , 22.40 22.60 22.80 23.00 23.20 m/z 189.20 14.98%

Of 66 80 *4 mmmmmmmmmp lll 160 ill......^l .... , ,

mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188 P 22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 10.47%

80 94 SB ...... . .......................... .................................................... 01 ■ ■ i ■ “ ■ i ■1' ■ i ■ ■1' i • ■1 ■

n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 . r i ... I .... I . 1(18 22.40 22.60 22.80 23.00 23.20 m/z 80.05 9.97%

5000

80 94 160 66 0 nmmpp -r ....। I I।। । । . ■ i ■ ■ ■ ' i ■ • ITi . । । । । . /z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

31644.D SCAN508.M Tue Jan 22 08:37:19 2002 Page 13

NYC-WTC_000050006

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GCMS analysis results for sample AD31670, Jan 28 2002 · Box DEP Box 28

NYC-WTC_000050008

Laboratory report showing GCMS analysis of sample AD31670 including unknown compounds and surrogate recovery data.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996