GCMS analysis results for sample AD31644, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31644 including unknown compounds and surrogate recovery data.

NYC-WTC_000049990–000050007

Folder label: “GCMS X 1/3/02 A 1/17/02”

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NYC 9/11 Public Portal Document Llbrary searen compound Keporc Data File : C:\MSDCHEM\1\5973N\02JAN17\31644.D Vial: 4 • Acq On : 17 Jan 2002 5:19 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Phenanthrene, 9-methyl- $$ ... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 99241 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 2 Bitoscanate 192 C8H4N2S2 004044-65-9 59 3 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 53 4 1,2-DI(3-THIENYL)ETHENE 192 C10H8S2 013640-84-1 53 Abundance Scan 1656 (22,280 min): 31644.D (-) m/z 192.10 100.00% 1912

5000 / 1 _ 70 82 | 96 | 120 146 Id 160 22.00 22.20 22.40 22.60 0 » I » » J 44 II» • I hmpp— • • । ■! “ • ■।‘। ‘।11 “ ••। । ■ m/z 191.10 15.43% m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 19/2

5000 ........ P ■ ■ i ■ * ■ ■ । ■ • • ■ । 22.00 22.20 22.40 22.60 ■ A m/z 193.10 14.52% 96 165 88 J 139 152 j 176 , , 0 " i1 ■ “ i “ ■ ■ i " • ■ r • ■ ‘ i1 ■'11 • I" ■ i “ 1111 “ ■ i “ “ i “ ' '’I' " 11111111,1 ‘ 111111 “ i I 4-rrp-r /z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102102: Bitoscanate 1912 i I I । t II* i n i p r » 11 22.00 22.20 22.40 22.60 5000 m/z 82.10 12.81% 134 90 160 64 76 1102, 49—nupTmanmumama 0 TIm—nn 176 Ipun—*p miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102107: 1,2-Phenylene diisothiocyanate . ......... A...... M 1912 22.00 22.20 22.40 22.60 m/z 146.10 12.40% 64 5000-

75 90 134 l h l 160 107 0 mijlhn]..... " I ‘■ ■ i • lladyan ■ ■ i “ “ i ■ miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ■ >i “ “ । ।|> p ■ ■ > । i ' ‘ i" ............. A 11 — T1 j 31*1 22.00 22.20 22.40 22.60

31644.D SCAN508.M Tue Jan 22 08:37:19 2002 Page 12

NYC-WTC_000050005

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GCMS analysis results for sample AD31670, Jan 28 2002 · Box DEP Box 28

NYC-WTC_000050008

Laboratory report showing GCMS analysis of sample AD31670 including unknown compounds and surrogate recovery data.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996