Laboratory report documenting GCMS analysis of sample AE11278 conducted on May 22, 2002, including surrogate recovery data.
NYC-WTC_000024692–000024705Folder label: “GCMS X 5/13/02 A 5/15/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Llbrary searen compound keport
Data File : C:\MSDCHEM\l\DATA\020515\11278.D Vial: 12 Acq On : 15 May 2002 10:41 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 2,4-Diamino-6-(hydroxymethy... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.08 0.34 ug/1 35951 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2,4-Diamino-6- (hydroxymethyl) pte. . . 192 C7H8N60 000945-24-4 59 2 3-Amino/7-methyl-1,2,4-benzotria... 192 C8H8N4O2 1000213-87-8 43 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 40 4 3-(2-Mqthoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 40 Abundance Scan 4766 (31.082 min): 11278.D (-4754) (-) m/z 192.10 100.00% 192
5000
146 1 1 i ■ ' TAAAP——— 44 66 82 96 160 30.80 31.00 31.20 31.40
m/z-> mrprrye ■ 111 ■ > ■ fl l /1 pt > r 11 > r 1111 —11 10 20 30 40 50 60 70 80 90 100110120130140150 160 170180190 200 mHI ll.... '" I' rn/z 146.10 19.18% Abundance #125821:2,4-Diamino-6-(hydroxymethyl)pteridine 43 192 163
5000 1 1 I ' 1 ‘ ‘ I ' ‘ 1..... 28 30.80 31.00 31.20 31.40 53 68 146 175 m/z 96.20 17.47% 77 92 106 121 133 , tiglssjailp tl pin 4i 11 rh nodpposgapos ll/ . ■ rlll i, । rl " I'"' i ’T’ n/z-> 10 20 30 40 50 60 70 80 90 100110120130 140150 160170180190 200 Abundance #80865:3-Amino-7-methyl-1,2,4-benzotriazine 1,4-dioxide 192 1 AA— 30.80 31.00 31.20 31.40 5000 m/ z 82.10 14.34% 65 150 89 176 42 51 i, 77 104 121 131 --। nl 11 mll nimonn’... . 4159.. .7 TT- n/z-> Abundance 10 20 30 40 50 60 70 80 90 100110120130140150 160 170180190 200 #81034: Anthracene, 2-methyl- 192 1.41.14... 1,, 30.80 31.00 31.20 31.40 m/z 193.00 13.02% 5000
82 96 165
m/z—> 18 27 39 51 69 | ll 115 126 139 152 „| 176 „ i < | < > j 1111 ' 1111 i'| 1111 |'i 111 [ I ri 111I'ri 11111!'] 11 Tri 111 , ‘ 111111 [ 1111'| 1111 "I i । rll 11 । i*| 11 it i i
10 20 30 40 50 60 70 80 90 100110120130 140150 160 170 180190200 iii it 4 30.80 31.00 31.20 31.40
11278.D SCAN020507.M Thu May 16 09:56:22 2002 Page 7
NYC-WTC_000024702
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NYC-WTC_000024706
Laboratory report documenting GCMS analysis of sample AE11281 conducted on May 22, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024730
Laboratory report documenting GCMS analysis of sample AE11280 conducted on May 22, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024652
GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025568
GCMS analysis report for sample AE11567 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024871
Laboratory report of GCMS analysis for sample AE10246 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025580
GCMS analysis report for sample AE11568 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025542
Laboratory report documenting GCMS analysis of sample AE11154 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025520
Laboratory report of GCMS analysis for sample AE10812 conducted on May 29, 2002, showing surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024896
Laboratory report of GCMS analysis for sample AE10247 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025613
GCMS analysis report for sample AE11571 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024915
Laboratory report of GCMS analysis for sample AE10301 conducted on May 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
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Laboratory report documenting GCMS analysis of sample AE11305 conducted on May 28, 2002, including surrogate recovery data.
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NYC-WTC_000024629
Laboratory report showing blank test results for GCMS analysis of sample AE11157 conducted between May 13 and May 16, 2002.
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Laboratory report displaying calibration data for GCMS analysis of sample AE11157 conducted between May 13 and May 16, 2002.
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NYC-WTC_000024644
Laboratory report displaying reference standard results for GCMS analysis of sample AE11157 conducted between May 13 and May 16, 2002.
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