GCMS reference results for sample AE11282, May 2002

NYC 9/11 Public Portal Document Llbrary searen compound Report

Data File : C:\MSDCHEM\1\DATA\020516\11282.D Vial: 10 Acq On : 16 May 2002 6:16 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 Phenanthrene-diO Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

31.96 0.35 ug/1 26758 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1Phonanthrenc dl 0 188 C14D10 001517-22-2 91 2 Anthracene-d10- 188 C14D10 001719-06-8 83 3 Phosphonic acid, (3-methyl-3-pen. . . 188 C8H1303P 022152-34-7 59 4 Pyrrolo [2,3-b] indole, 1,2,3,3a, 8 . . . 188 C12H16N2 004089-16-1 40 Abundance 1 Scan 4915 (31.958 min): 11282. D (-4906) (-) m/z 188.20 100.00% 118

5000

80 94 31.60 31.80 32.00 32.20 49 11"1111 ■" r । " i" 1 'i11 ‘ i -HH 114... 132....... 160........ 1 | 66 ■ ।1' " ।1'' 1111" ।' 111'' (' " 11' । ।' 11111'1 m/z 80.10 19.14% n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 ,.................... 31,60 31.80 32.00 32.20 80 m/z 94.10 18.35% 94 160 30 42 52 66 ,, 11 108118 132 146 II 170179,1,1 TT"ImmHuhutt I I I 1 | I I I I | I 1. I ! I I I I | I I I I | Tl-t-l | I l-l'l1!'! I I I | I I I ! | |l|'llll| , | , I miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1(8

31.60 31.80 32.00 32.20 5000 m/z 189.20 12.67%

80 17 30 42 52 66 94 160 .1 1ITTTI . ।. 11 > 111111. ■ 11»। --HHH । 108 118 132 146 I 170179,i 11111i1111 ■ 111111111111111111111 IT|'i 111111 ii । itI1 Tuur n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79704: Phosphonic acid, (3-methyl-3-penten-1-ynyl)-, dime... 1(8 31.60. 31.80 32.00 32.20 m/z92.10 12.43% 5000 77 62 35 47 91 109 155

m/z—> pAf.AeuLellpl. ‘II 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 P— 128 141 . । 11111 111 111111 ii ' 173 ITT’ p-TTT ■ I ’ ■ > i-]' ' । । r i । ' । । I ' 31.60 31.80 32.00 32.20 । ।

11282 .D SCAN020507.M Thu May 23 09:42:20 2002 Page 5

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