GCMS results for sample AE11481, May 29, 2002

NYC 9/11 Public Portal Document LiDrarY searen compound Report

Data File : C:\MSDCHEM\l\DATA\020521\11481.D Vial: 15 Acq On : 21 May 2002 10:11 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 6 Phenanthrene-diO Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.37 ug/1 38828 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 45 2 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 43 3 Anthracene-d10- 188 C14D10 001719-06-8 40 4 Pent^cyclo[7.3.1.1. (4,12).0(2,7)... 188 C14H20 1000215-61-8 40 Abundance Scan 4914 (31.952 min): 11481 .D (-4906) (-) m/z 188.20 100.00% 188

5000 94 160 ............................... ................... 66 78 31.60 31.80 32.00 32.20 42 261 miz-> 0- m TIT60 20 40 ----- __ i 80 100 120 140 160 ‘II 180 200 220 240 260 I m/z 94.10 33.55% Abundance #79827: Phenanthrene-d10 188

5000 31.60 31.80 32.00 32.20 80>94 m/z 184.10 32.34% 160

m/z-> 0 +28 40 52.6644.1108120132 146 l. 20 40 60 80 100 120 140 160 180 200 220 240 260 * ’ iY ’ ’ ’ i ’ * ' ' i 1 ‘

Abundance #79714: Pentacyclo(8.4.0.0(3,7).0(4,14).0(6,11 )tetradecane 188 .......................... ...........................

31.60 31.80 32.00 32.20 ____ 5000 m/z 160.20 22.00% 79 91 41 „ 67 105117 131 145 159 173 0- IB27 T ia v । > II, I ri । * niz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #79826: Anthracene-d1 0- ■ ■ i ■ 1 ' ' i ■ 108 31.60 31.80 32.00 32.20 m/z 92.10 21.65% । < | /_ i -r । r i i i । । 5000

80 94 160 , 28 40 52 66 —1-106118,132,146..- ' I*' ■ । O1' 11 1 1 ' 1 1 l~ ' 1,1 । । । ■ n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 31,60 31.80 32.00 32.20

11481.D SCAN020521.M Fri May 24 09:37:18 2002 Page 8

NYC-WTC_000022586