GCMS results for sample AE11481, May 29, 2002

NYC 9/11 Public Portal Document LIDrdLY bearcr compound xeporc

Data File : C:\MSDCHEM\l\DATA\020521\11481.D Vial: 15 Acq On : 21 May 2002 10:11 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 5 Anthracene, 2-methyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.10 0.27 ug/1 27875 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 64 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 3 Phenanthrene , 1-methyl- 192 C15H12 000832-69-9 53 4 Thiophene, 2-[2-(3-thienyl) ethen. . . 192 C10H8S2 116854-09-2 53 Abundance Scan 4769 (31.100 min): 11481 .D (-4758) (-) m/z 192.10 100.00% 192

5000

n/z-> Noundance 0 k4a,5trzO.”?.ubrz.ls.1 mHH 20 30 40 50 60 70 80 90 100110120130140150160170180190200210220 #125845: Anthracene, 2-methyl- T-p-T 214 ----- 30,80 31,00 31.20 31.40 m/z 191.20 24.68%

192

5000 ■ ■ i ■ ■ i ■ • 30.80 31.00 31.20 31.40 m/z 193.00 19.17% 66 75 87 96 115 126 139 152 105 176 0 ‘ I " 1' I " " r ’'' I ’ " " 11 l'h r‘ I'l'i r" r I pri. | ili . 11 .'| 1.11. ..... Ml 11. rh | ■. .'I1 ‘’"I""!'... lz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Noundance #81033: Phenanthrene, 9-methyl- 192

30,80 31,00 31.20 31.40 5000 m/z 160.10 16.06%

29 39 51 63 74 83 T 115 126 139 152 165 176 || 0 TTWTTTTTPTTTpt ■ ■ i ■' ■ ■ ■ ■ 1' ■ ■ i 1 m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #125856: Phenanthrene, 1-methyl- 1 ■ i ' ■ ■ • i ‘ ' 1 i ‘ ' ■ i ■ ■ 19/2 30,80 31.00 31.20 31.40 m/z 96.20 14.52% 5000

96 4PE n/z-> 27 39 51 63 0 TUm—TThhHt 82 1 115 126 139 152 190 178 । 20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 220 lttp 1 1 1 1 1 1 1 1 1 • i ■ ■ ■ ' i ■ ' 30.80 31.00 31.20 31.40

11481.D SCAN020521.M Fri May 24 09:37:16 2002 Page 7

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