GCMS results for sample AE11481, May 29, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11481.D Vial: 15 Acq On : 21 May 2002 10:11 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Methylene Chloride Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 28.90 0.25 ug/1 26379 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methylene Chloride 84 CH2C12 000075-09-2 27 2 Chloroiodomethane 176 CH2C1I 000593-71-5 16 3 Methylene /Chloride 84 CH2C12 000075-09-2 16 4 Methylene/Chloride 84 CH2C12 000075-09-2 16 Abundance 1 Scan 4395 (28.902 min): 11481 .D (-4384) (-) m/z 243.90 100.00% 49 209 244

86 173 5000 102 136 229 75 28.60 28.80 29.00 29.20 0- • 1 i ■ ■ ‘ 1 i ■ • ' 1 i ■ ■ i ■ ■ ■ 1 । * > i ■ ■ ■ 1 i ■ ■ ’ I ’d. . t I TI , ( t r. . I m/z 208.80 84.12% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #111039: Methylene Chloride 49

84 5000 1 1 ■ i 1 ■ 1 1 i ‘ 28.60 28'80 29.00 29.20 m/z 49.00 82.77%

01 — 35 ,+71, *11 ■ ■ ■ ■ । I 0000/00000000000000001/ niz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #111042: Chloroiodomethane 49

28.60 28.80 29.00 29.20 5000 m/z 207.00 74.43% 127 176 141

miz-> 0- +24 20 364 40 60 75 91 80 113 J 162 1’1 ' ■ ■ i ' ■ I....... . 100 120 140 160 180 200 220 240 Abundance 49 #12327: Methylene Chloride AALLAL 1 28.60 28.80 29.00 29.20 101

84 m/z 173.10 53.30% 5000

35 0 14 TTIn +— 70 . i < l • > ■ • । i T-T-p-r-r-r-p-r ■ 1 1 1 1 1 I 1 1 1 1 I nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 28.60 28.80 29.00 29.20

11481.D SCAN020521.M Fri May 24 09:37:15 2002 Page 6

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