GCMS analysis results, Sample AE08267, April 22, 2002

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GCMS analysis report for sample AE08267 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048421–000048435

Folder label: “GCMS X 4/9/02 A 4/17/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08267.D Vial: 24 Acq On : 18 Apr 2002 4:22 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 Anthracene, 2-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.33 ug/L 573667 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 2 Anthracene, 9-methyl- 192 C15H12 000779-02-2 40 3 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 40 4 Anthracene, 2-methyl-________________ 192 C15H12 000613-12-7 40 Abundance Scan 3330 (22.645 min): 08267.D (-3323) (-) m/z 192.10 100.00% 19 2

A 5000

96 146 ‘ I‘ 160

n/z-> 0+ 11" " I" " I' 20 30 42 52 40 THHH 70 82 qil " I "118 132 ' । I । ' ' ' I । " ' I ' I' 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 -l+n , 1111111111 4. 22.40 22.60 22.80 m/z 191.10 23 00 22.94% Abundance #125847 Anthracene, 2-methyl- 152

— 5000 22.40 22.60 22 80 23.00 m/z 146.10 16.44% Q6 1 AS 28 39 51 63 74 82 . 115 126 1 39 1 52 1 176184 | 0 TITTTTUUTTTCTTTTTTTTTTTTTUTTTTLTTTDTWTLWWLWTTTTTTHTTTTT Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125848: Anthracene, 9-methy- 152

22.40 22 60 22.80 23 00 5000 m/z 193.10 14.61%

27 39 51 63 74 82 1 96 115 126 139 152 0 176 165 0 ' i111 ■ r ■ •' r TPTPr ri r 1-| | | l r ! ■ 1*1 I | I I I I | I I ■ r*| > ■ r < |*I ■ ■ ■ | 141 I | I I I l ] n H ‘I’T ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81041 Phenanthrene, 3-methyl- 192 2240 22.60 22.80 23.00 m/z 96.00 13.64% 5000

96 63 74 82 .1 115 126 139 152 165 176 27 39 51 0 TIPIWIptnum | I', " | ' l l I I'l'i rl | I N I I’! ! ! , | I ri | | I | | | ...... . . . . I , I | — ...... 1111 '‘i1 " I" n/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.40 22.60 22 80 23.00

08267.D 041702SCAN.M Thu Apr 18 10:01:02 2002 Page 7

NYC-WTC_000048431

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NYC-WTC_000048431Source: NYC Law Department, mirrored locally

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