GCMS analysis results, Sample AE08263, April 22, 2002

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GCMS analysis report for sample AE08263 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048333–000048354

Folder label: “GCMS X 4/9/02 A 4/17/02”

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Data File : C:\MSDCHEM\1\DATA\020417\08263.D Vial: 20 Acq On : 18 Apr 2002 1:07 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Anthracene, 2-methyl- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.28 ug/L 318935 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 64 2 Anthracene, 1-methyl- 192 C15H12 000610-48-0 59 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 50 4 Phenanthrene, 2-methyl-_____________ 192 C15H12 002531-84-2 50 Abundance Scan 3330 (22.645 min): 08263 D (-3322) (-) m/z 192.10 100.00% 19 2

5000

96 160 ■ ■ । ■ V........ 1 ‘ ‘ ■ I ' ' ' ' I 40 70 82 22.40 22 60 22.80 23 00

n/z-> 0 HHSRL H 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 — ।II I|I |||||,,!। ■■ |II m/Z 191.00 27.64% Abundance #125845: Anthracene, 2-methy- 19 2

5000 22.40 22.60 22.80 23.00 m/z 193.00 18.00% 96 165 , 67 75 88 । 115 126 139 152 I 176 0- ............................. 1 ■ I’li . .... 1' i'l r i111 r ............. 1..... 11'"' i r’th 11 'I' 1''1111 TITT n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125855: Anthracene, 1-methyl- 102

22.40 22.60 22.80 23.00 5000 m/ z 146.10 15.50%

165 no I 27 39 51 63 74 87 96 | 178 ' 115 126 139 152 n/z-> o- 11UWIWTTTTTITPPTTT I ■ ■ ■ ■ ‘I " ■ ■ . . hipurfpirdp+r 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TITT

Abundance #81033: Phenanthrene, 9-methyH- 11 192 22 40 22 60 2280 23.00 m/Z 96.00 15.25%

5000

96 165

n/Z-> 29 39 51 63 75 83 l 115 126 139 152 | 176 0 ' i " " i " " i11" I " " i11'11' i1 ■ ■111 "111" ............ ............. I'....... ’ti TPTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ll—p 2240 22.60 22.80 23.00

08263.D 041702SCAN.M Thu Apr 18 09:51:16 2002 Page 15

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GCMS analysis results, Sample AE08264, April 22, 2002 · Box DEP Box 27

NYC-WTC_000048355

GCMS analysis report for sample AE08264 showing surrogate recovery and unknown compound screening on April 22, 2002.

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