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GCMS analysis results, Sample AE08263, April 22, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08263 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048333–000048354

Folder label: “GCMS X 4/9/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08263.D Vial: 20 Acq On : 18 Apr 2002 1:07 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98. L ********************************************************************* Peak Number 11 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.54 ug/L 606927 Phenanthranene-dl0 23.02

Hit# Of 5 Tentative ID MW MolForm . CAS# Qual

1 Phenanthrene-dlO 001517-22-2 72 188 C14D10 2 Anthracene-dl0 - 001719-06-8 72 188 C14D10 3 4H-Pyrido[1,2-a]pyrimidin-4-one,. 057773-19-0 50 188 C11H12N2O 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 Abundance Scan 3420 (23 174 min): 08263.D (-3414) (-) m/z 188.10 100.00% 188

5000

80 94 juna23.00 22.80 — 23.20 23.40 23.60 i 1 ■ 1 ■ i ■

43 57 66 132 160 0 ................. . ----- TTTTTTTT m/ Z 94.10 16.50% n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-dlO 188

5000 '■r I"UDnTI 1 1 TI . " ' ‘I" 22.80 23.00 23.20 23.40 23.60 m/ z 189.10 14.10% 80 94 160 30 42 52 66 |I h ।102110118 132 146 | 170 180 0 I ■1 " ............."I.......... . H ।, I 111 ■ ■ il b r . I | | I I i I | I I n | I I । । | I I I i | I I I I | I rll’P । 'I IT I I I | l'l‘l Tur n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

22.80 23.00 23.20 23.40 23.60 5000 m/ z 80.05 13.01%

80 94 160 66 17 30 42 52 .102 118 132 146 ,i| 170 180 0 I" " 111' '111 ■ '11 ■ ■ ■ I111' 11t*NnNmTtt fm-r n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance itlQllG'. 4H-Pyrido[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- ) V 1 । ' n 1 1 ' 7 ' ' ' ' 1 1 145 188 22.80 23 00 23.20 2340 23.60 173 m/z 184.05 12.96%

5000 92

65 39 119 132 159 I 55 I Tp 0 ------ 78 । .I ।। , , . .................. 1............ I,, 'I 1 |i 11. 1‘‘‘1 '' I'''' I " " 11' " I ’1 • Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23 00 23.20 23.40 23.60

08263.D 041702SCAN.M Thu Apr 18 09:51:18 2002 Page 16

NYC-WTC_000048352

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