GCMS results for sample AE08070, Apr 2002

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Laboratory report documenting GCMS analysis of sample AE08070 including surrogate recovery and unknown compounds on April 18, 2002.

NYC-WTC_000046855–000046863

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \MSDCHEM\1\DATA\020415\08070.D Vial: 27 Acq On : 16 Apr 2002 8:02 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.35 ug/L 353175 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Phenanthrene-dl0 188 C14D10 001517-22-2 90 2 Anthracene-dlO- 188 C14D10 001719-06-8 80 3 4H-Pyrido[1,2-a]pyrimidin-4-one ,. 188 C11H12N2O 057773-19-0 40 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 33 Abundance Scan 3420 (23 174 min) 03070.D (-3414) (-) m/ z 188.40 100.00% 108

5000

94 66 80 160 22 80 23 00 23 20 23.40 23.60

TT/Z-> 0 i■ ■ । H ■ i'1'■i 49 —mmmmmHH "’i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 18 9.40 17.31% Abundance #79827: Phenanthrene-d10 188

5000 2280 23.00 23.20 23.40 23.60 80 m/z 94.25 16.89% 94 160 30 42 52 66 ■ I 102110118 132 146 1 170 180 0 IITTHTH 1111 [ I »i 11111111111111 1111111 rff । 111111 11ini n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d IQ- 188 _______M -p-r ■ i * * ■ ■ । L 22.80 23.00 23 20 23.40 23.60 5000 m/ z 184.30 13.18%

80 94 160 , I 66 [ ■ ■ 11, ।. n 11. ।t. — । 170140—— 17 30 42 52 1102 118 132 146 0-rmarp I ! । | III! | I I I I | । । I I —H || ■■" 111" n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79770: 4H-Pyndo[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- i 1 1 ■ 1 i 145 188 22 80 23.00 23.20 2340 2360 173 m/z 92.30 11.51%

5000 92

65 39 159 I 55 , HI 0- ----- 78 | 119 132 ............... | ‘IT ‘ ‘ITTTTTTETTETTTITTI’T 1,711174. 111" T’unr . .... R /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22 80 23 00 23 20 23.40 23.60

08070.D 041202SCAN.M Tue Apr 16 13:58:51 2002 Page 4

NYC-WTC_000046862

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