GCMS analysis results for sample AE08251, April 2002

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Laboratory report documenting GCMS analysis of sample AE08251 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047772–000047801

Folder label: “GCMS X 4/8/02 A 4/17/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\DATA\020417\08251.D Vial: 9 Acq On : 17 Apr 2002 4:02 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 18 Phenanthrene-dlO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 23.18 0.69 ug/L 933659 Phenanthranene-dlO 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual ( Phenanthrene-dlO 188 C14D10 001517-22-2 83 2 Anthracene-dlO- 188 C14D10 001719-06-8 72 3 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 45 4 Cycloheptanone, 4-phenyl-188 C13H160 067688-28-2 37 Abundance Scan 3420 (23 174 min) 08251 D (-3413) (-) m/z 188.10 100.00% 188

5000

2 1 40 22.80 23 00 23.20 23 40 23.60 57 66 80 132 146 158 III 0 ...................... b't, ,|i hi, 1.11.H | , ■ 11,1 ■ I. ■ 11 r ■ 111..... 10011j5mp TV m/z 189.05 15.49% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79327: Phenanthrene-d10 188

5000 22.80 23.00 23 20 23 40 23 60 80 m/z 184.05 13.97% 94 160 30 42 52 66 1 102110118 132 146 | 170 180 0 • 11.1 ■ 11' ■. । ■ ■|1 < ■ ■ 11 ■ 11 ■ | <11 " ■ 11 11 < । | I 11 । | | | 11 | I | 11 111 I 11 ■ i I i 11 iTr|.........TTTttnr n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826- Anthracene-d10- 188 ,.......... 22.80 23.00 23.20 23.40 23.60 5000 m/z94.05 13.48%

80 94 160 , I 17 30 42 52 66 /z-> 0 ' i1 ■ " i " " 1111111 mrntt । < 111111 J 102 118 132 146 + Tmmmpototn 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 +170.180,. Abundance #79791: Benzene, 1-(1-cyclohexen-1-yl)-4-methoxy- .......... / 1 I ' ' 1 ' TT—.—TT 188 22 80 23 00 23 20 23.40 23 60 m/z40.00 12.23% 5000 160

115 129 145 173 7 91। 102 41 51 65 77 0 ------------- - 1 llpt+ll TTJU /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23 20 23.40 23 60

08251.D 041702SCAN.M Thu Apr 18 09:12:18 2002 Page 23

NYC-WTC_000047798

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