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GCMS blank results for volatile organics, April 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank analysis results for volatile organic compounds in sample AE08260 from April 2002.

NYC-WTC_000048225–000048255

Folder label: “GCMS X 4/9/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\0409LB.D Vial: 4 Acq On : 17 Apr 2002 11:51 am Operator: Nefliu Sample : 04/09 1b Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Phenanthrene-dlO Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 23.18 0.93 ug/L 1039960 Phenanthranene-dl0 23.02 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 52 2 Anthracene-dlO- 188 C14D10 001719-06-8 49 3 Tridecane 184 C13H28 000629-50-5 38 4 Eicosane, 10-methyl-________________ 296 C21H44 054833-23-7 25 Abundance Scan 3421 (23 180 min)' 0409LB.D (-3413) (-) m/z 188.10 100.00% 188

57 5000 43 71 85 94 1 ' I ' k ' I Tin 160 22.80 23 00 23 20 23 40 23 60 , ,1 113 132 0 -HHm T-pT m/ z 57.10 62.68% /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827 Phenanthrene-dlO 168

AWuAsonZ. 5000 22.80 23 00 23 20 23.40 23.60 80 m/z 71.10 44.45% 94 160 30 42 52 66 | 102110118 132 146 0 TPTTHTTH 11PP . ................... n/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 10— 22.80 :23.00 23 20 23.40 23.60 5000 m/z 43.10 43.78%

nn 80 94 160 0 17 30 42 52 ° PPWTTTTTTTTTTTTT | I 102 118 132 146 Tur +,.179.189. Z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #16403: Tridecane A/ WAoonu 43 57 22 80 23 00 23 20 2340 23 60 m/ z 85.10 26.82% 71 5000 29 85

n/Z—> 0l.. -"H' —l Ipomipan) 127 141 155 TTTTTTT ' r '1 ■ i " 99 113 184 " r " 1 r 1" r" 1 r1" I " 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 AA].. HU* 22.80 23.00 23 20 2340 23.60

0409LB.D 041702SCAN.M Thu Apr 18 09:42:00 2002 Page 13

NYC-WTC_000048240

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NYC-WTC_000048240Source: NYC Law Department, mirrored locally

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