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GCMS analysis results for sample AE07974, April 18, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07974 conducted on April 18, 2002.

NYC-WTC_000047564–000047576

Folder label: “GCMS X 4/4/02 A 4/15/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020415\07974.D Vial: 14 Acq On : 15 Apr 2002 9:26 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Phenanthrene-dlO Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 23.17 0.37 ug/L 467457 Phenanthranene-dlO 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual (1 Phenanthrene-diO 188 C14D10 001517-22-2 72 2 Anthracene-d10- 188 C14D10 001719-06-8 50 3 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) .. . 188 C14H20 1000215-61-8 43 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 Abundance Scan 3420 (23 174 min): 07974 D (-3414) (-) m/z 188.40 100.00% 168 A

5000

22 80 23 00 23.20 23.40 23.60

/z-> 0 .pa?.pbtC.li. I'1" I 132 10 TTuuttgur 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 184.30 13.66% Abundance #79827 Phenanthrene-d10 188

5000 22 80 23 00 23 20 23 40 23.60 80 m/z 189.35 13.63% 94 160 30 42 52 66 ll 102110118 132 146 ,11 170 180 0 nWmTTTTTTH TTgTTTDTPTTTTTT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 TT I ' ' ' ' I ' 22.80 23 00 23 20 23.40 23.60 5000 m/z 92.30 11.18%

80 94 160 , i 66

n/z- > 17 30 0-TUTwuuuptrr 42 52 m+ ! —170.189— Pteutn 118 132 146 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3 1 1 (4.12).0(2,7) 0(6.11 )tetradeca... ' ' | 'V■ T| I I I I | I 1 I I | I 188 22 80 23 00 23.20 23.40 23.60 m/ z 80.30 10.16% 5000 79 91 55 67 105 0 117 131 n/z-> llll JI 0 ' i " " i " " r " ' i' ll 145 159 71.173, Ju .Ml..'.1!1!'... L ■i111 ■ i"' <r1 > .......... ..... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22 80 23.00 23.20 23.40 23.60

07974.D 041202SCAN.M Tue Apr 16 13:44:36 2002 Page 8

NYC-WTC_000047575

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NYC-WTC_000047575Source: NYC Law Department, mirrored locally

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