GCMS analysis results for sample AE08066, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE08066 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046786–000046798

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\DATA\020415\08066.D Vial: 23 Acq On : 16 Apr 2002 4:47 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 23.17 0.34 ug/L 368733 Phenanthranene-dl0 23.02 . Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 90 2 Anthracene-dlO- 188 C14D10 001719-06-8 90 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 Abundance Scan 3420 (23 174 min) 00066 D (-3413) (-) m/z 188.40 100.00% 18 8

5000

- 80 94

n/z-> O-TTTTT —# 43 57 66132 158 ll. I 11 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TT m 22.80 m/z 23 00 23 20 94.30 23 40 23 60 16.40% Abundance #79827 Phenanthrene-d10 18 8

5000 ........... / 22 80 23 00 23 20 23.40 23.60 80 m/z 189.30 14.43% 94 160 30 42 52 66 132 146 ll 102110118 1 170 180 o ■ ।■ 11 "'I'"' I"" I1"' 1111'I" I' I" । 11 I I । 11 । i: 111 111 । 11 11 । | i n । rm-[ । .. ........... .. 11 i i r’l’l’I 1 । । TT n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 18 8

22 80 23 00 23 20 23.40 23.60 5000 m/z 80.30 13.84%

80 94 160 . 66 17 30 42 52 1 .1 102 118; 132 146 ,|| 170 180 । 0- TOTIUWTTTTTTTTTTHTmH "11 n11111 111,11.. . TVTTWTTTTTTTT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771 3-Amino-4-methyl-6-methoxyquinoline 188 22.80 23.00 23 20 23 40 23.60 m/z 184.30 12.27% 145 5000

117 01. | | || | 41 51 63 77 89 102 130 , ‘h . |■|ll'|■| | ||l|l|-| y#/h . I rt. ! 4 . | I rIl I I ■■|^|■| . . . | ill [ , 159 173 , -mm /Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22 80 23 00 23 20 23 40 23.60

08066.D 041202SCAN.M Tue Apr 16 13:55:44 2002 Page 8

NYC-WTC_000046796

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NYC-WTC_000046796Source: NYC Law Department, mirrored locally

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GCMS results for sample AE08069, Apr 2002 · Box DEP Box 27

NYC-WTC_000046841

Laboratory report documenting GCMS analysis of sample AE08069 including surrogate recovery and unknown compounds on April 18, 2002.

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