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GCMS analysis results for sample AE08066, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting the GCMS analysis of sample AE08066 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046786–000046798

Folder label: “GCMS X 4/5/02 A 4/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08066.D Vial: 23 Acq On : 16 Apr 2002 4:47 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Phthalic acid, diisooctyl e... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.46 0.24 ug/L 227247 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2 38 2 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 17 3 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 12 4 4-Pyridinecarboxaldehyde, 3-hydr... 167 C8H9NO3 000066-72-8 9 Abundance Scan 4830 (31 458 min)' 08066 D (-4822) (-) m/z 149.20 100.00% 149 40

227 5000 57 167 71 | 83 114 __ _ ,1, ...... 31.20 31.40 31.60 31.80 0+ ’i ■ ■ ■ ■ 11 .... I....... I ............ PPmm 240 1 1 I 1 ' ■ • I ' 1 ' ■ I ' 1 ’ ■ I ’ ' • ' I 1 ' 1 ' 1 1 ' ' ' I ' m/z 40.20 79.93% n/z- > :20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #66787 Phthalic acid, diisooctyl ester 149

5000 57 167 31 20 31.40 31.60 31.80 43 71 m/z 227.40 52.80% I l 1 83 07 113

n/z—> 20 0 .97+4124 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #123456 1,2-Benzenedicarboxylic acid, mono(2-ethylhexy!) .. 149

31 20 31.40 31 60 31 80 5000 m/z 57.30 39.56% 70 57 167 41 83 112 - ...................... 279 . 0+ 'J....... n/z-> Abundance 20 40 60 80 100 160 180 200 220 240 260 120 140 #67064, 1,2-Benzenedicarboxylic acid, mono(2-ethylhexylj este 149 280 M... 11. 31.20 31 40 31 60 31.80 m/z 167.20 36.02% 5000 70 167 41 55 83

n/Z- > 29111 +-1,4.87 1.4,132 0 TIT T’’ 1T1 TEi P 20 40 60 80 100 112

120 185 199 213 228 242 256 278 i ’ 11 ■ i ■ “ ' ■ i ' ■ ' ■ i • ' ■ ■ i ' 1 ■ ' i ' 1111..... 1 1 1 140 160 180 200 220 240 260 280 31 20 31 40 31 60 31 80

08066.D 041202SCAN.M Tue Apr 16 13:55:44 2002 Page 9

NYC-WTC_000046797

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NYC-WTC_000046797Source: NYC Law Department, mirrored locally

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