GCMS results for sample AE07766, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \MSDCHEM\1\DATA\020415\07766.D Vial: 28 Acq On 16 Apr 2002 8:51 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 15 Didodecyl phthalate Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.46 0.39 ug/L 394228 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Didodecyl phthalate 502 C32H5404 002432-90-8 14 2 Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2 12 3 2,7-Octadienoic acid, ethyl este... 168 C10H16O2 055282-91-2 7 4 4-Pyridinecarboxaldehyde, 3-hydr... 167 C8H9NO3 000066-72-8 5 Abundance Scan 4830 (31 458 mm): 07766.D (-4817) (-) m/z 227.40 100.00% 227

k 149

5000- 57 95 167 70 84 109 123 TIT ■ • i ■ • 43 31 20 31.40 31.60 31.80 O-* 11 m/z 149.20 96.64% "ddl ‘ 1 ।7 n/z—> 20 40 60 80 100 120 140 160 180 200 220 Abundance #66779 Didodecyl phthalate 149

57 5000 31 20 31 40 31.60 31 80 m/z 57.30 38.81% 69 83 1 04 wMby,/Maaaly, 123133 167 i. H — 0— ■ i ’ • ■ ""i — ■n/z—> 20 40 60 80 100 120 140 160 180 200 220 Abundance #66787: Phthalic acid, diisooctyl ester 149

31 20 31.40 31 60 31.80 5000- m/z 95.30 31.99%

AHlpAyaMMArMWwh— 57 167 43 71

0— J JU 1 i83"I ■ 95■' ‘14 i104113122 132 I " 1 1 • l’1 1 r 1 TI ' i ' 1 1 1 i ■ ■ ■ 1 i ■ ■ 1 1 i ■ 1

n/z- > 20 40 60 80 100 120 140 160 180 200 220 Abundance #456: 2,7-Octadienoic acid, ethyl ester. (E)- 23 55 81 31.20 31.40 31.60 31 80 95 41 m/z 167.20 31.99% 67 5000- 123 114 140

168

/Z— > 0- 20 —l L 60 80 qlulqlulqll 100 120 —140I_ 160 180 200 220 ■ i ■ ' 31 20 31 40 31.60 31.80 ‘ I’*

07766.D 041202SCAN.M Tue Apr 16 13:42:17 2002 Page 18

NYC-WTC_000046886