GCMS analysis results, Sample AE08269, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08269.D Vial: 25 Acq On : 18 Apr 2002 5:10 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Phthalic acid, diisooctyl e... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

31.45 0.25 ug/L 380431 Chrysene-dl2 30.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phthalic acid, diisooctyl ester 390 C24H38O4 001330-91-2 25 2 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 23 3 Tricyclo[3.3.1.13,7]decanone, 4-... 228 C10H13BrO 032456-49-8 22 4 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 17 Abundance Scan 4829 (31.452 min): 08269 D (-4816) (-) m/z 149.00 100.00% 149 227

5000 167 57 113 43 I 71 i 1 ' ' ■ i 31.20 31.40 31.60 31 80 I 84 99 , 0 — 14.4.1. 207 [ 240 m/z 227.20 74.15% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #66787 Phthalic acid, diisooctyl ester 149

5000 IT 57 167 31 20 31.40 31.60 31.80 43 71 m/z 167.00 38.07% — 83 Q7 113

n/z-> 20 0+ 40 60 — 74132— 80 100 120 140 160 180 200 220 240 260 280 Abundance #67064: 1,2-Benzenedicarboxylic acid. mono(2-ethylhexyl) este 149

31 20 31.40 31 60 31.80 5000- m/z 57.10 28.11% 70 167 29 41 55 83 112 0+412744 —T) 132 185 199 213 228 242 256 278 n/z-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 #66944 Tricyclo[3 3.1.13,7]decanone, 4-bromo-, (1.alpha.,... 121 149 260 280 1 M 31.20 31.40 31.60 31.80 m/z 113.50 26.74% 79 5000 67 93 55 |...4111,0.7 228 0 - 11....... 1..... ...... .................. 4... Tl/Z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 31 20 31.40 31.60 31.80

08269.D 041702SCAN.M Thu Apr 18 10:02:31 2002 Page 15

NYC-WTC_000048454