GCMS analysis results for unknown compounds, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\060702\12739.D Vial: 15 Acq On 7 Jun 2002 7:58 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 19 Phthalic acid, diisooctyl e... Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 31.33 0.27 ug/L 223321 Chrysene-dl2 30.76 Hit# Of 5 Tentative ID MW MolForm CAS# Qual l Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2/ 59 2 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-/ 50 3 Tricyclo[3.3.1.13,7]decanone, 4-... 228 C10H13BrO 032456-49/8 25 4 1,3-Benzodioxole-5-(5-oxo-pentan... 236 C12H1205 1000146-55-6 9 Abundance Scan 4808 (31.329 min): 12739.D (-4802) (-) m/z 149.00 160.00% 149

5000 167 43 57 70 227 83 113 , 240 31.00 31.20 31.40 31.60

miz-> ol TTT1 :20 UM TLt ■ ■ i1 ‘ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ i ■ • ■ • i ■ —— m/z 167.00 39.81% 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #66787: Phthalic acid, diisooctyl ester 149

5000 57 167 31.00 31.20 31.40 31.60 43 71 m/z 57.10 31.00% — 83 — 113 132 Ol miz-> ;20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #67064:1,2-Benzenedicarboxylic acid, mono(2-ethylhexyl) este 19 I 111 31.00 31.20 31.40 31.60 5000 m/z 70.10 28.89% 70 167 29 41 55 83 112 0!TIT —4+4MJ T— 185 199 213 228 242 256 278 miz-> 120 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #66944: Tricyclo|3.3.1.13,7]decanone, 4-bromo-, (1.alpha.... 121 149 31,00 31.20 31,40 31.60 m/z 227.10 27.77% 79 5000 67 93 N

miz-> 0 20 l 41 55

40 60 80 . I . PP ■ 1 j t t 1 ■ । rnr

100 120 140 160 180 200 220 240 260 280 228

■ ' i ■ ■ ■ ■ i • ■ 31.00 31.20 31.40 31.60 ■ ■ i ■ ■ 1 1 i

12739.D 060302.M Mon Jun 10 11:51:16 2002 Page 22

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