Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.
NYC-WTC_000043938–000043957Folder label: “GCMS X 4/25/02 A 5/7/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\050602\9968.D Vial: 25 Acq On 7 May 2002 7:14 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e
Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Phthalic acid, diisooctyl e... Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
31.38 0.27 ug/L 240396 Chrysene-dl2 30.81
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2 50 2 Tricyclo[3.3.1.13,7]decanone, 4-.. 228 C10H13BrO 032456-49-8 27 3 Furo[3,2-b]pyridine, 2-methyl-, .. 149 C8H7NO2 069022-83-9 16 4 3-Azabicyclo[3.3.0]octane, 7-iso.. 227 C16H21N 1000156-34-6 9 Abundance Scan 4817 (31.382 min): 9968. D (-4812) (-) m/z 149.05 *0.00% 40 149
227 5000 167 .............. ........................................ 57 71 113 240 31.00 31.20 31.40 31.60 31.80 , , 84 ||....................................................... 1 > । > । r—i pi । i ■ । । । . i । > i ■ p1 m i—। > > । ' । > -- m/ z 40.10 96.79% m/z->_______ 40 60 80 100 120 140 160 180 200 220 240 Abundance #66787: Phthalic acid, diisooctyl ester 149
5000 TT 1387 57 167 31.00 31.20 31.40 31.60 31.80 43 71 m/z 227.10 51.61% 83 — 113 , id.,1d,t 60 80 | 97,1 123133 ' ' | "I I r 'I1 | r I” I1 I 100 120 | I I I 1 । 140 i 1 | 1 i । i 1 । 160 1 । 180 < i 1 > । 200 i >. । 220 । 1 ' i i | ' 240 m/z-> 40 । Abundance #66944: Tricyclo[3.3.1.13,7]decanone, 4-bromo-, (1.alpha.... 121 149 11 ' I 1 ' 1 1 I ' ' 79 31.00 31.20 31.40 31.60 31.80 5000 m/z 167.10 41.30% \ 67 93 41 55 228 > ■ । i > 1 ,I 1 1 l80 .mmm 100 120 140 160 180 200 -PL 220 —240— lz-> 40 60 Abundance #66755: Furo[3,2-b]pyridine, 2-methyl-, 4-oxide "I 149 31 00 31.20 31.40 31.60 31.80 m/ z 57.20 32.56%
5000 A 43 == KG 104 120 133 1155 66 78 1 ' i T ■|""1 1 1 1 । 1 1 i 1 1 1 1 i 1 1 ' ■ 1 1 ' 1 1 i 1 1 ■ ■ i ■ > । ■ i ■ 1 ■ ■ । । । ■ 1 ■ i ■ ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 31.00 31.20 31.40 31.60 31.80
9968.D 050102.M Tue May 07 15:47:03 2002 Page 12
NYC-WTC_000043954
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000043958
Laboratory report for sample AE09969 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043919
Laboratory report for sample AE09967 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044926
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10199 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043976
Laboratory report for sample AE09970 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044994
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10204 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044071
Laboratory report for sample AE09971 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045171
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10308 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044885
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10198 on May 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044001
Laboratory report for sample AE09972 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045137
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10306 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045155
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10307 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045075
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10303 conducted on May 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000043745
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 25 and May 7, 2002.
Filed in the same folder
NYC-WTC_000043746
Fragmented page containing Method 508 headers and partial text from a DEP laboratory record dated April 2002.
Filed in the same folder
NYC-WTC_000043749
Laboratory report documenting a method blank analysis for GC/MS testing of volatile organic compounds from May 2002.
Filed in the same folder
NYC-WTC_000043756
Calibration data report for sample AE09684 listing response factors and concentrations for target analytes in May 2002.
Filed in the same folder
NYC-WTC_000043760
Reference gas chromatography-mass spectrometry analysis with manual result entry for sample AE09684, detecting multiple organic contaminants.
Filed in the same folder