GCMS analysis results, sample AE09974, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9974 .D Vial: 22 Acq On 7 May 2002 4:48 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 Phthalic acid, diisooctyl e... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.38 0.23 ug/L 222974 Chrysene-dl2 30.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2 53 2 1,2-Benzenedicarboxylic acid, mo.. 278 C16H2204 004376-20-9 50 3 Didodecyl phthalate 502 C32H5404 002432-90-8 3. 4 Tricyclo[3.3.1.13,7]decanone, 4-.. 228 C10H13BrO 032456-49-8/37 Abundance Scan 4817 (31.382 min): 9974. D (-4808) (-) m/z 149.00 100.00% 149

5000 57 167 227 41; , 71 ®

m/z-> ||197 113 207 । 240 4 kt.l T-1 iii t l । । । । । । ir । । I r' । । | I । I I | 1 r i । i i i" i । i i > r-] i m । । । lii — 1 i 1 1 ' 1 i ' 1 20 40 60 80 100 120 140 160 180 200 220 240 260 280 t 31.00 31 20 31.40 31.60 31.80 m/ Z 57.10 34.50% Abundance #66787: Phthalic acid, diisooctyl ester 149

5000 43 57 71 167 A 1 । ' ■ 1 1 i ■ ' ' * rr 1 1 1 । ' 1 ' 1 i 1 1 31.00 31.20 31.40 31.60 31.80 m/z 167.00 33.98% 83 113 97 ll 132 | i ' ‘ ■ 1 i 1 1 lz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #67064: 1,2-Benzenedicarboxylic acid, mono(2-ethylhexyl) este 14.9 1....A। i । । i ।

31.00 31.20 31.40 31.60 31.80 i i । i । । । । r i 1 1 1 ■ i ■ 1

5000 m/Z 227.10 28.54% 70 167 41 cc 29157 h, 87 I1 ■. 1,132 . 83 112 185 199 213 228 242 256 278 "FTddnprvrrTi |* I' I I I I l"'l I I 1" I > । । । । । । । i । i । । । । । i । । । । । । । n F i r m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #66779: Didodecyl phthalate । | I I I I | I । 1 I | I T1 I | | I I I 1 I ' J' I " I 149 31.00 31.20 31.40 31.60 31.80 m/ z 41.10 22.27%| 57 5000

m/z--> I 1 "’"I 11 I 83.104.133 20 40 60 69 02 Ti ItI । ’ III | r I I

80 100 I | I

120 ।rn|I

140 Til 167 ll L! I I I ' I I Cl’m

160 180 200 220 240 260 280 I I I I I I I l ' I I 1 1 I I I I I ...... 31.00 31.20 31.40 31.60 31.80 II... 1 i 1 1

9974.D 050102.M Tue May 07 15:53:28 2002 Page 8

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