GCMS analysis results, sample AE09974, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\l\DATA\050602\9974.D Vial: 22 Acq On 7 May 2002 4:48 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Carbamic acid, methylnitros... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 34.94 0.24 ug/L 165567 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Carbamic acid, methylnitroso-, e.. 132 C4H8N203 000615-53-2 3 2 Adenosine, 2-methyl- 281 C11H15N5O4 016526-56-0 1 3 1,10-Diaminodecane 172 C10H24N2 000646-25-3 1 4 1-Octanamine 129 C8H19N 000111-86-4 1 Abundance Scan 5423 (34.942 min): 9974.D (-5421) (-) m/z 40.10 10 0.00%| 43

5000 208 281 86 132 i i । i i i । । i i i i । i t i 1—[—r 263 34.60 34.80 35.00 35.20 —I 4 i | i i i । | 1 r 116 ' i 1 1 1 1 i 1 ' TIu—vnIu I I I I I I I I [—r ■ 1 i 1 1 1 1 I 1 1 1 1 r1 1 1 1 r 1 m/ z 36.10 48.59% m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #108023: Carbamic acid, methylnitroso-, ethyl ester " I A 3 I |lt|l ll ill l| lip 5000 43 57 34.60 34.80 35.00 35.20 m/z 208.00 47.58% .1 73,86 132 ■ ■ i ■ ' m/z->______ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #1079: Adenosine, 2-methyl- 31 Ah AAAar. MA/rk/HO 34.60 34.80 35.00 35.20 5000 45 m/z 281.10 39.52% 59 74 149 178

ti/z—>______ 20 —Hl 80 100 120 140 160 180 200 220231240251264 40 60 87 281 108 133 || 163 | 192 206 I | r i 1 । । r । r । । ITUt । । ii । । । । । । । i i I i । T"i “i‘ i । । i । । ।11 । 'i । । r r1 r n |* । i 260 280 Aa Abundance #108170:1,10-Diaminodecane 1, Tfil 33 34.60 34.80 35.00 35.20 m/ z 85.90 30.24%|

5000

| 44 II, I 69ii । 86I 100 114 128 143156 ■ 11. Lill । I I 4 । 1 | ' । ' * ] 1 । 1 I | ' । । । | > । । I | | I I । | ' I ।| ' I I I | I I I I | I I I I | I I I I | I I I 'I | I I I T |____ I I I I MAQAAA,L MAA,AAMAAA/44MM n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 __ 3460 34.80 35.00 35.20

9974.D 050102.M Tue May 07 15:53:28 2002 Page 9

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