GCMS analysis report, sample AE07568, April 2002

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Laboratory results for unknown compounds and surrogate recovery in sample AE07568 analyzed on April 9, 2002.

NYC-WTC_000047195–000047215

Folder label: “GCMS X 4/2/02 A 4/3/02”

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Data File C:\MSDCHEM\l\DATA\020403\07568.D Vial: 16 Acq On 3 Apr 2002 10:56 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 1-(3,4-Methylenedioxybenzyl... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

42.16 0.24 ug/1 178961 Perylene-dl2 42.30 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-(3,4-Methylenedioxybenzylidene... 207 C9H9N3O3 1000224-56-9 5 2 Methyl 2-methyl-2-(methoxy-3-hyd... 221 C9H19NO5 1000143-85-8 4 3 9-Octadecenamide, (Z) - 281 C18H35NO 000301-02-0 3 4 Adenosine, 2-methyl- 281 C11H15N5O4 016526-56-0 3 Abundance Scan 6652 (42.163 min): 07568. D (-6645) (-) m/ z 73.10 100.00% 73 147

5000 221 207 281 41.80 42.00 42.20 42.40 01 11111‘17‘/‘‘+‘*‘‘I‘‘‘‘I‘‘•‘#‘1*1)‘‘‘‘I‘lI‘I1+‘1111111‘‘‘I‘IIW 111171 fi । m/z 147.10 69.08% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #65807:1 -(3,4-Methylenedioxy benzy lidene)semicarbazide 4|4 147

63 76 207 163 5000 41.80 42.00 42.20 42.40 105 121 134 m/z 221.10 43.74% .ill1 । 90

m/z-> 0 ' ' T‘ ■ 1 'T1 20 40I + +l —1 60 80 100 120 140 160 180 200 220 240 260 280 11190. 1..................

Abundance #15294: Methyl 2-methyl-2-(methoxy-3-hydroxypropoxy)amino-... 5)6 ....... II......... 41.80 42.00 42.20 42.40 5000 73 m/z 207.00 28.58% 30 88 102 120 162 221 ... 146 190 206 n/z-> 0 20 40 TT 60 h—80 100 120- il l ‘I1rr111111111111111111/0TT"1/ITTu/T 140 160 180 200 220 240 260 280 Abundance #109752: 9-Octadecenamide, (Z)- 'i 1 1 ' "It 1 1 1 1 1 TI* 1 1 ' 1 1 43 59 41.80 42.00 42.20 42.40 m/z 281.00 25.47% 5000 72 29 16 , I, 1 97 122 0 k kubeh 193,207221,236....... 281, m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 41.80 42.00 42.20 42.40

07568.D SCAN020403 ,M Thu Apr 04 10:30:38 2002 Page 7

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