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GCMS analysis report, sample AE07520, April 2002

Machine-extracted title · confidence 100%

Laboratory results for volatile organic compounds in a GCMS blank sample analyzed on April 2-3, 2002.

NYC-WTC_000047159–000047176

Folder label: “GCMS X 4/2/02 A 4/3/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020403\0402LB.D Vial: 10 Acq On 3 Apr 2002 5:21 pm Operator: Nefliu Sample 04/02 lab blk Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 3-Isopropoxy-1,1,1,5,5,5-he .. . Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 41.58 0.53 ug/1 387721 Perylene-dl2 42.30 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,5,5,5-hexamet.. . 354 C12H3404Si4 072182-11-7 9 2 Silanamine, N-[2,6-dimethyl-4-[(. . . 281 C14H27NOSi2 072088-09-6 5 3 9-Octadecenamide, (Z)- 281 C18H35NO 000301-02-0 4 4 Methyl 2-methyl-2-(methoxy-3-hyd... 221 C9H19N05 1000143-85-8 4 Abundance Scan 6553 (41.582 min): 0402LB.D (-6537) (-) m/z 147.05 100.00% 73 147 221 281 5000 355

1 1 1 ' 1 ' 1 1 ' 1 ' 1 1 1 1 ' 1 ......... . 1 1 1 41.20 41.40 41.60 41.80 42.00 m/ Z 73.05 93.48%

A mz-s 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #27710: 3-lsopropoxy-1,1,1,5,5,5-hexamethyl-3-(trimethylsi... 73 281 43 5000 207 1 i ■ ■

339 41.20 41.40 41.60 41.80 42.00

A m/z 281.00 64.35% 190 — 0 1'lTI1 ' I II . 133 i । l'i । i i"l i rri । rti r163 .. 229265, 1 297 .. -n-p mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #27716: Silanamine, N-[2,6-dimethyl-4-[(trimethylsilyl)oxy... 73 281 ■ i ' ■ 266 41 20 41.40 41.60 41.80 42.00

A 5000 m/z 221.10 63.67% 45 251 179

4 127179 X 147 236 | 0 ' • I ‘11' I'' - ’ I • ’ 1 ■ i1 ■1 ■ i' ■ 1’111111111111111171111 ■ ■ i''' ■ r 1111111 ■ i' /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #113302: 9-Octadecenamide, (Z)- ■ i ■ • 41 20 41.40 41.60 41.80 42.00 m/z 355.00 47.39%

5000 41 A 83 98 126 281

n/z-> 0 —444444+13419184199.22277 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 41.20 41.40 41.60 41.80 42.00

0402LB.D SCAN020403 .M Thu Apr 04 10:14:25 2002 Page 7

NYC-WTC_000047168

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