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GCMS analysis report, sample AE07568, April 2002

Machine-extracted title · confidence 100%

Laboratory results for unknown compounds and surrogate recovery in sample AE07568 analyzed on April 9, 2002.

NYC-WTC_000047195–000047215

Folder label: “GCMS X 4/2/02 A 4/3/02”

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Data File C:\MSDCHEM\l\DATA\020403\07568.D Vial: 16 Acq On 3 Apr 2002 10:56 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 10 4-(3-Dimethylaminopropoxy)b... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

43.44 0.20 ug/1 144990 Perylene-dl2 42.30 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-(3-Dimethylaminopropoxy)benzal... 207 C12H17NO2 026934-35-0 3 2 2-1-Phenyl ethylidene-hydrazono-... 281 C16H15N3S 1000148-55-3 3 3 2-Hydroxyphenyl pyrrolidinyl thione 207 C11H13NOS 084783-01-7 2 4 lH-Pyrrole-2,5-dione, 1-(4-chlor... 207 C10H6C1NO2 001631-29-4 2 Abundance Scan 6870 (43.444 min): 07568.D (-6863) (-) m/z 281.00 100.00% 281

5000 73 207

147 43.20 43.40 43.60 43.80 0- m/z 207.00 32.42% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #18335: 4-(3-Dimethylaminopropoxy)benzaldehyde 58

5000 43.20 43.40 43.60 43.80 m/z 73.10 31.14%

n/z-> 0 ,15,29.42. ,, , , 77 92 105 121 i ' 1 '■ ‘I‘‘ItTtturu 20 40 60 80 100 120 147 180 200 220 240 260 280 140 160 207 I....... I'1 ' ' 1 1 TTT

Abundance #97319: 2-1-Phenyl ethylidene-hydrazono-3-methyl-2,3-dihyd... 281 ANY,.......... .MA,I , | 43.20 43.40 43.60 43.80 5000 m/z 147.00 4.65% 77 150 109 136 163

0- ■ i ' 1 ■ ■ i ■ 63.1 91 1122 ,, I I| ........223i....252 ■ ■ i ' ■ ■ 'i ■ ■■ 11 fi ■। ■ ■ 266 I... । . i' ' ' ' i 1 ' 1 1 i1 ■ ’ ' i 1 ■ ■ ■ i ' ■ ■ 1 i 1 ' 1 ' i 1 r ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #24189: 2-Hydroxyphenyl pyrrolidinyl thione 7b 43.20 43.40 43.60 43.80 207

137 5000

120 55 0 ...... | 93 . 174/ ,190T । JI1 ...... /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280

07568.D SCAN020403.M Thu Apr 04 10:30:39 2002 Page 12

NYC-WTC_000047210

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