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GCMS analysis report, sample AE07568, April 2002

Machine-extracted title · confidence 100%

Laboratory results for unknown compounds and surrogate recovery in sample AE07568 analyzed on April 9, 2002.

NYC-WTC_000047195–000047215

Folder label: “GCMS X 4/2/02 A 4/3/02”

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Data File C:\MSDCHEM\l\DATA\020403\07568.D Vial: 16 Acq On 3 Apr 2002 10:56 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 11 Adenosine, 2-methyl- Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.

43.48 0.19 ug/1 139126 Perylene-dl2 42.30 Hit# of 4 Tentative ID MW MolForm CAS# Qual 1 Adenosine, 2-methyl- 281 C11H15N5O4 016526-56-0 2 2 Furfurylideniminosulphur pentafl... 221 C5H4F5NOS 090598-15-5 1 3 2(3H)-Thiazolimine, 3-hydroxy-4-... 273 C9H8C1N3O3S 058275-70-0 1 4 Furo[3,4-b]furan-2 ,6(3H,4H)-dion... 266 C15H2204 020223-76-1 1 Abundance Scan 6875 (43.474 min): 07568.D (-6873) (-) m/ z 40.10 100.00% 43

5000

221 281 43.20 43.40 43.60 43.80 0TTT 147 I m/z 221.10 16.31% /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #1079: Adenosine, 2-methyl- 31

5000 45 59 74 ii 43.20 43.40 43.60 43.80 m/z 281.00 12.65% 1 „ " " . 149 178 86 .198120133, . 1 163 . J . 192 206 I 53 239251 264 281 OT biL 4dhurni"" /z—> 20 40 60 80 100 120 140 160 180। 200 220 240 260 280 Abundance #1230: Furfurylideniminosulphur pentafluoride 39

94 43.20 43.40 43.60 43.80 5000 m/ z 147.00 3.99% 66 127 51 221 I 202 | 0 I 1 ' ' 'I ‘ ‘‘I ' ' ' ' I ' ' ' ' I ' 1 1 1 I 1 1 1 1 v 1 1 > | 1 > I 1 I I I 1 1 I' < 1 I 1 (■ < > > I | I > | TTV ‘ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #1208: 2(3H)-Thiazolimine, 3-hydroxy-4-(3-nitrophenyl)-, m... 33 43.20 43.40 43.60 43.80 221

5000 175 89 51 64 76 104 121133 148160 192 . 237 OT 14 444 .4 । , ------- 111 ' 1 i Ii1 ■ 1 ,■1 j ■ ■ ■ ■ ) । 1 । i|1 । /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280

07568.D SCAN020403.M Thu Apr 04 10:30:39 2002 Page 13

NYC-WTC_000047211

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