GCMS blank results for volatile organics, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\0409LB.D vial: 4 Acq On : 17 Apr 2002 11:51 am Operator: Nefliu Sample : 04/09 1b Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 17 Adenosine, 2-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

35.10 1.13 ug/L 967888 Perylene-dl2 34.78

Hit# of 3 Tentative ID MW MolForm CAS# Qual

1 Adenosine, 2-methyl- 281 C11H15N5O4 016526-56-0 3 2 3-Aminooxy-4-chlorobutyric acid,... 181 C6H12C1NO3 1000186-78-9 1 3 Hexafluoro-1,5-pentanediol 212 C5H6F6O2 000376-90-9 1 Abundance Scan 5450 (35 101 min): 0409LB D (-5449) (-) m/z 40.00 100.00% 40

5000 57 149 71 123 209 260 85 97 0—r ■ ■ I ■ .1 1. 1 ■ r 11 1 1 ■ i ' ' ■ ■ i 1 1 II 281 • ■ i1 1 ■ m/z 34 80 35 00 35 20 35 40 57.10 36.25% /Z-> Abundance 20

31 40 60 80 100 120 140 160 180 200 #1079: Adenosine, 2-methyl- 220 240 260 280

,/"yhnat 5000 45 34 80 35 00 35 20 35.40 59 74 149 1 78 m/z 41.00 31.14%

n/z--> 04, ■ ■ i ■ 1

Abundance 20 40

29 -mm . 60 , 86 239251 264 281 108-120133 | 163 I 192 206 80 100 120 140 160 180 200 220 240 260 280 #591 3-Aminooxy-4-chlorobutyric acid, ethyl ester | T I | I 1 V, 'I ri'T | | I ! ! ! |' | | y4"w"MM/anipr 121 85 34 80 35.00 35.20 35.40 41 5000 m/z 149.00 31.14% 103 // 136149

Ti/Z--> Abundance 0—r ■ ■ i ■ 20 uulu“7Z1u 40 60 80 -44—4 100 120 140 j 165 181 160 180 #1054: Hexafluoro-1,5-pentanediol 200 220 240 260 280

31 34.80 35.00 35 20 35.40 m/z 141.10 21.93% 5000

142 16 49 61 77 95 111123 | | .162175 193 ... ............ 0—147-4-44 n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34 80 35.00 35.20 35.40

0409LB.D 041702SCAN.M Thu Apr 18 09:42:03 2002 Page 24

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