GCMS blank results for volatile organics, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\0409LB.D Vial: 4 Acq On : 17 Apr 2002 11:51 am Operator: Nefliu Sample : 04/09 1b Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L ********************************************************************* Peak Number 18 5-Bromo-2-mercaptopyridine-... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

35.22 0.98 ug/L 839253 Perylene-dl2 34.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 5-Bromo-2-mercaptopyridine-l-oxide 205 C5H4BrNOS 1000211-96-6 35 2 Morpholine, 4-acetyl- 129 C6H11NO2 001696-20-4 11 3 Phenol, 6-methyl-2-[(4-morpholin... 207 C12H17NO2 060460-71-1 9 4 Phosphine, cyclohexyl(1,1-dimeth... 186 C11H23P 074685-81-7 9 Abundance Scan 5470 (35 219 min): 0409LB.D (-5466) (-) m/z 43.10 100.00% 43

5000 57

86 98 129 207 281 /MHMys, 150

/z- > 0 ।

Abundance 20 .... 40 . i < । । ‘‘‘0" 60 L 444 I I I.. 69

80 ,111 * ‘ । ■1' ■ । 100 120 140 160 180 200 220 #84853: 5-Bromo-2-mercaptopyridine-1-oxide 167

• ■ ,-n * -11 • 1 ■ i 1 ■ 1 ■ i ■ ■ 240 263 I 260 280 34.80 35.00 m/z 57.10 / I ' 1 ' ' 1 1 '

80.08% ■ ■ i ■ 35 20 35.40 35 60

207

82 109 45 5000 TB" Tf 157 34 80 35.00 35.20 35 40 35 60 57 69 95 190 m/z 280.90 55.18%

n/z-> 0 ___ L i1 ■ ■ ■ I 144

20 40 60 LLL 41/44, ula, 1 26 1.11175 44MP,... .।, 80 TT 145

100 120 140 160 180 200 220 240 260 280 Abundance #16367: Morpholine, 4-acety- 57 43 34 80 35.00 35.20 35.40 35.60 5000 86 129 m/z 207.00 52.19%

0 29 4 I 44 — 72 99 A Auuapayouos n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #84739: Phenol, 6-methyl-2-[(4-morpholiny!)methyl} I ' ' ' ■ I ’ ' ' 1 I 207 34 80 35.00 35 20 35 40 35.60 86 m/z 49.00 49.80%

n/z-> 5000

0 - 20 ' ir 40 41

60 57 419.4 80 I

100 120 121

134 , 140 160

AI , 1175 190 । / 160 180 200 220 240 260 280 MM**** 34.80 3500 35.20 35.40 35.60

0409LB.D 041702SCAN.M Thu Apr 18 09:42:03 2002 Page 25

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