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GCMS analysis report sample AE09679, May 23, 2002

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GCMS laboratory report for sample AE09679 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013224–000013250

Folder label: “GCMS X 5/21/02 A 5/21/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052102\9679.D. Vial: 17 Acq On : 22 May 2002 2:22 am Operator: Mclean Sample : re-extract Inst : Insttumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 5-Bromo-2-mercaptopyridine-... Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 5.37 0.25 ug/L 159399 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 5-Bromo-2-mercaptopyridine-l-oxide 205 C5H4BrNOS 1000211-96-6 38 2 2-Methyl-7-phenylindole 207 C15H13N 001140-08-5 9 3. 6-Methyl-5-[1-piperidinyl] -2,4-p... 207 C10H17N5 1000212-53- 9 4 N-Methyl-1-adamantaneacetamide 207 C13H21NO 1000211-60/4 9 Abundance Scan 390 (5.371 min): 9679.D (-385) (-) m/z 207.00 100.00% 207

5000 49 35 58 84 133 191 0 44Ll++ L n/z—> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 500 m/z 5.20 49.10 5.40 5.60 5.80 30.75% Abundance #84853:5-Bromo-2-mercaptopyridine-1-oxide 2(7

82 109 45 5000 157 500 5.20 5.40 5.60 5.80 57 69 95 190 m/z 58.10 20.26% 119

m/z—> 0-pr4 A 44 44 + +4 + 4444 Mawl +3.44. 20 30 40 50 60 70 80 90 100110120130140.150160170180190200210 1466175,.. tmlm Abundance #84866:2-Methyl-7-phenylindole 207

500 5.20 5.40 5.60 5.80 5000 m/z 43.10 19.53%

30 41 51 63 77 88 102 115 130-139 152 165 178 191 MMMatwoojoy O rui ’ * ■. I'. .T. । I’m . r’l , I ■ r’ rt , । Pl 111 i AT,,, ,11. |'I.. lin.. llp irja rl i ■ ■" miz—> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #84786:6-Methyl-5-[1 -piperidinyl]-2,4-pyrimidinediamine 207 5.00 5.20 5.40 5.60 5.80 m/z 209.00 17.84% 150 5000 43 124 138 55 69 81 q« 108 O-p . TIItT . . . . . . . , Tt ,—p „ 165 178 189 | . , . Tt ■ ■ "i'A । joihi Wpos ।. M .I., miz—> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 5.00 5.20 5.40 5.60 5.80

9679.D 052202.M Wed May 22 11:45:33 2002 Page 15

NYC-WTC_000013243

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NYC-WTC_000013243Source: NYC Law Department, mirrored locally

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