GCMS analysis report sample AE09679, May 23, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052102\9679.D Vial: 17 Acq On : 22 May 2002 2:22 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 1,3,5-Cycloheptatriene Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 4.27 1.63 ug/L 1032010 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 25 2 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2/9 3 Cyclobutene, 2-propenylidene- 92 C7H8 052097-85-/ 9 4 Bicyclo[3.2.0]hepta-2,6-diene 92 C7H8 002422-86/8 5 Abundance Scan 202 (4.266 min): 9679.D (-198) (-) m/z 91.10 100.00% 91

5000-

49 __________ 65 38 , | 82 4.00 4.20 4.40 4.60 0- --------- , , ,l,I,........... Il, , , * i ■ ■ ■ • i■■■■i 11 1 ■ I m/z 92.10 59.34% Tl/Z-> 0 10 20 30 40 50 60 70 80 90 100 110 Abundance #37276:1,3,5-Cycloheptatriene 91 M 5000 ■ ■ i • ' ■ ■ i ' ' I ‘ ' I ‘ ' 4,00 4.20 4.40 4.60 39 65 m/z 49.10 21.14% 27 2 15 0- ' 1 i1 ■ 1 • i • ■■ ■ i ■ - 45.71,57,4171,77.85. 106 niz-> 0 10 20 30 40 50 60 70 80 90 100 110 Abundance #117298:1,3,5-Cycloheptatriene 91 4.00 4.20 4.40 4.60 5000 m/z 65.10 15.94%

39 65 28 | 45 51 TJ 85 , 0- }‘*I* eg ——1. 1**11 niz-> 0 10 20 30 40 50 60 70 80 90 100 110 Abundance #37324: Cyclobutene, 2-propenylidene- 91 4.00 4.20 4.40 4.60 m/z 50.00 11.89% 5000

39 65 MMA"AW/WKMsty 27 1 45 51 77 0 ' । I ‘ ‘ ‘ I 1 ' ' CT' ' 1 1 i ' ' rlttee’i i l'1'i i . ’’ill i [ i i ,’i । i i i 11 1 ' i ■ • ■ ■ i ■ ■ niz-> 0 10 20 30 40 50 60 70 80 90 100 110 4,00 4.20 4,40 4.60

9679.D 052202.M Wed May 22 11:45:31 2002 Page 14

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