DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB27\02386.D Vial: 2 Acq On : 27 Feb 2002 4:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 4 1,3,5-Cycloheptatriene $$ C... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 4.38 0.07 ug/L 38993 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3,5-Cycloheptatriene $$ Cycloh... 92 C7H8 000544-25-2 64 2 1,3,5-Cycloheptatriene (CAS) $$ ... 92 C7H8 000544-25-2 9 3 METHYLFULVENE 92 C7H8 000000-00-0 9 4 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 9 Abundance Scan 89 (4.378 min): 02386.D (-) m/ z 91.05 100.00% 91

5000 M 41 50 65 85 4.00 4.20 4.40 4.60 4.80 0+ 7/ m/z 92.10 67.03% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5570:1,3,5-Cycloheptatriene $$ Cyclohepta-1,3,5-triene $... 91

5000 ....... 1 i ' ‘ 1 ' i ■ ' ■ 1 i ■ ■ ■ ■ i ■ ■ ■ ' i ' 4.00 4.20 4.40 4.60 4.80 65 m/ z 65.10 8.66% 27 38 A miz- > 46.7l4l4., 0+ ■ ■ i ■ ■ ■ ■ r ■ l ■ ■ i1 ■ ■11 ■ 11 ■ । ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 ■ ।1 r ■ ■ ।11 > ‘ । < ।। ■111 1 ■ ।11 ■11' ■

Abundance #5568:1,3>5-Cycloheptatriene (CAS) $$ Cycloheptatriene $$... 91 4.00 4.20 4.40 4.60 4.80 5000 m/ Z 63.00 8.40%

39 _ 65 61 , | 86 0+ 111'1 " i " " i'' " I''111 1" " i ■ ■r ‘ i ‘ ' i ■ " 1111111" " 111111" 11111" I " 111 1' i " " I'' m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5531: METHYLFULVENE 91 4.00 4.20 4.40 4.60 4.80 m/z 85.10 7.80%

5000

39 65 I 45 61, ।, 0 HIPPTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 4.00 4.20 4.40 4.60 4.80

02386.D HP022102.M Thu Feb 28 08:47:09 2002 Page 6

NYC-WTC_000005035