GCMS analysis report for sample AE01510, March 2002

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GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010027–000010046

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report .• Data File : C:\MSDCHEM\1\5973N\02FEB21\01510.D Vial: 5 Acq On :. 21 Feb 2002 2:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 1,3,5-Cycloheptatriene (CAS... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 4.38 0.07 ug/L 32697 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3,5-Cycloheptatriene (CAS) $$ ... 92 C7H8 000544-25-2 64 2 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 40 3 ETHINYLCYCLOPENTENE- (1) 92 C7H8 000000-00-0 9 4 METHYLFULVENE 92 C7H8 000000-00-0 9 Abundance Scan 89 (4.378 min): 01510.D (-) m/z 91.00 100.00% 91

5000

■ । ■ ■ ■ ■ । ■ i ■ ■ • ■ । ‘ i ■ 45 65 4.00 4.20 4.40 4.60 4.80 Of - m/z 92.00 56.82% miz-> 20253035404550556065 70 75 80859095 100 Abundance #5568:1,3,5-Cycloheptatriene (CAS) $$ Cycloheptatriene $$... 91

5000 s 4.00 4.20 4.40 4.60 4.80 m/z 65.10 9.81% 39 65 J 61, | 86 0+ ■ ■ i" “ i ■ ■ • ■ i" TIi l FTr ri'. .. . I M . . | , ||I I I I I I H | I ■ I I | ! I I ! | 1 . I1| I II 1 | Hmp m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5569: 1,3,5-Cycloheptatriene 91 4.00 4.20 4.40 4.60 4.80 ‘ ■ I ■ ■ ■ ■ i ■

5000 m/z 45.20 7.16% 65 27 37 46 51 —1H— 01 “ i' ■ “ i ■1" i • ■ ■ • i •1 ■ • i “ ■ • i' ■ ■ ■ i1 ■ ■ ■ i • ‘ I “ “ I" " I ■" ‘ I" ‘ 11 " i1 •1 • i ■1 miz-> 2025303540455055 60 65 70 75 80 85 90 95 100 Abundance #5532: ETHINYLCYCLOPENTENE-(1) • i ■ ■ • • i ■ ■ i ‘ ' i ■ ■ ■ ■ i ' 91 4.00 4.20 4.40 4.60 4.80 m/z 43.10 6.60% A 5000 A 39 61,65 O ‘ • i" “ i' ■ ■ ■ i “ ■ ■ i ‘'111' “ ■ i “'ri'i11" i “ ■ ■ i1111111111111111"11' “11"111 111'1" i" I • ’ ‘ ‘ I • ‘ ‘I • ‘ ‘ ‘ m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 4.00 4.20 4.40 4.60 4.80

01510.D HP022102.M Mon Feb 25 10:55:09 2002 Page 6

NYC-WTC_000010036

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