GCMS analysis results, Feb 27 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB25\01136.D Vial: 3 Acq On : 25 Feb 2002 12:53 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L *************************** ** **************************************** Peak Number 4 1,3,5-Cycloheptatriene (CAS... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

4.39 0.08 ug/L 33763 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3,5-Cycloheptatriene (CAS) $$ ... 92 C7H8 000544-25-2 9 2 ETHINYLCYCLOPENTENE-(1) 92 C7H8 000000-00-0 9 3 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 9 4 lz3,5-Cycloheptatriene $$ Cycloh... 92 C7H8 000544-25-2 9 Abundance Scan 90 (4.390 min): 01136. D (-) m/z 91.00 100.00% 91

5000

51 4.00 4.20 4.40 4.60 4.80

n/z-> Of -Pp66. TT. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 11111111 m/z 92.00 56.86% Abundance #5568:1,3,5-Cycloheptatriene (CAS) $$ Cycloheptatriene $$... 91

5000 I' 1 1 ' i ' ’ 4.00 4.20 4.40 4.60 4.80 m/z 51.10 9.85% 39 . 65 .1 61 , । 86 /V A A 0 11'1" I ■ ■' ’ i'' ■1 r 11 M ''' ‘ 11'11111111'111111'111 ■1 TEWOmmmptutf PPP m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5532: ETHINYLCYCLOPENTENE-(I) 91 1 i 1 Tr i ■ ' ■ ■ i ■ ■ 4.00 4.20 4.40 4.60 4.80 5000 m/z 65.00 9.00%

39 61 65 0 ----- 1TRTTTTTT‘III*1 tiringr lz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5569:1,3,5-Cycloheptatriene 91 4.00 4.20 4.40 4.60 4.80 m/z 63.00 6.28%

5000

65 27 37 46 51 61, m/z-> 0 II1IWTIWT]NTTTITTTHTTT ■ i"'11 ■ " ■ i ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 +90 95 100 i ■11 ■ i 4.00 4.20 4.40 4.60 4.80

01136.D HP022102.M Tue Feb 26 08:29:56 2002 Page 6 NYC-WTC_000003453