GCMS analysis results for sample AD31647, Jan 25 2002

NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C: \MSDCHEM\1\5973N\02JAN22\31647.D Vial: 3 Acq On : 22 Jan 2002 1:51 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 1,3,5-Cycloheptatriene (CAS... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 4.37 0.14 ug/L 43179 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3,5-Cycloheptatriene (CAS) $$ ... 92 C7H8 000544-25-2 64 2 METHYLFULVENE 92 C7H8 000000-00-0 64 3 ETHINYLCYCLOPENTENE-(1) 92 C7H8 000000-00-0 9 4 Cyclobutene, 2-propenylidene-92 C7H8 052097-85-5 9 Abundance Scan 87 (4.367 min): 31647.D (-) m/ z 91.10 100.00% 91

5000’ 1 ■ i ■ ■ ■ ' i ■ ■ ■ ■ I ■ ■ ■ 1 I •

39 51 65 86 4.00 4.20 4.40 4.60 4.80 C TT-p-r-n-p-T m/z 92.10 59.15% miz-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5568:1,3,5-Cycloheptatriene (CAS) $$ Cycloheptatriene $$... 91

5000 ■ ■ i ‘ 1 ■ ■ i ■ ■ ■ ■ I ■ 1 I 11 11 I 1' 4.00 4.20 4.40 4.60 4.80 m/z 65.10 10.02% 39 65 61 , | 86 1 *14spu iz-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5531: METHYLFULVENE 91 ' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ 1 i ■

4.00 4.20 4.40 4.60 4.80 5000 m/z 39.10 9.34%

39 1 45 . 61 . 65 ।, I I I : I I I I I : n/z-> 3035 40 45 50556065 70 75808590 95 100 Abundance #5532: ETHINYLCYCLOPENTENE-(1) .......... ,11........... 91 4.00 4.20' 4.40 4.60 4.80 m/z 51.05 6.22% 5000 maj MWWyA 39 61 65 -h-p-n-rp-r ' ■ i ■ ' ■ ■ i ' ■ ■ ‘ i 1 ' ' ■ i ■ ■ • ■ i ■ iz—> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 4.00 4.20 4.40 4.60 4.80

31647.D SCAN508.M Thu Jan 24 13:55:40 2002 Page 5

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